Tetrahedron Letters p. 8439 - 8441 (1999)
Update date:2022-08-03
Topics:
Adinolfi, Matteo
Barone, Gaspare
Guariniello, Luigi
Iadonisi, Alfonso
Benzyl ether and benzylidene acetal carbohydrate protecting groups can be selectively cleaved by reaction with sodium bromate/sodium dithionite in ethyl acetate/water. Under the mild (room temperature, short reaction time) conditions needed, a variety of other protecting functionalities such as acetyl, chloroacetyl, benzoyl, pivaloyl, tosyl, t-butyldimethylsilyl, trityl, and isopropylidene groups remain unaffected.
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