Synlett p. 983 - 985 (1997)
Update date:2022-08-18
Topics:
Sugai, Takeshi
Hamada, Keiji
Akeboshi, Tomohiro
Ikeda, Hajime
Ohta, Hiromichi
Biocatalyst-mediated efficient preparation of highly enantiomerically enriched (R)-5-hexanolide (1) is described. The enantioselective reduction of 5-oxohexanoic acid with Yamadazyma farinosa IFO 10896 and the subseqent lipase-catalyzed kinetic resolution gave (R)-1 in 62% yield with 99.7% e.e.
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