Recueil des Travaux Chimiques des Pays-Bas p. 377 - 378 (1994)
Update date:2022-08-10
Topics:
Oda, Mitsunori
Kuroda, Shigeyasu
Shimao, Ichiro
Morita, Noboru
Asao, Toyonobu
The regioselective synthesis of dimethyl 1,3,5-cycloheptariene-1,2-dicarboxylate (4) was achieved by a ring expansion method, starting from dimethyl 1,3-cyclohexadiene-2,3-dicarboxylate (5).The title compound 3 was obtained as an air-sensitive oil by zinc-copper reduction of 1,2-bis(bromomethyl)cyclohepta-1,3,5-triene (10) to which the diester 4 was transformed.
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Doi:10.1080/10426500601015633
(2007)Doi:10.1139/v02-050
(2002)Doi:10.1016/j.chemosphere.2007.10.036
(2008)Doi:10.1016/j.molstruc.2020.128829
(2020)Doi:10.1039/CT9119900132
(1911)Doi:10.1021/jo00389a055
(1987)
