Recueil des Travaux Chimiques des Pays-Bas p. 377 - 378 (1994)
Update date:2022-08-10
Topics:
Oda, Mitsunori
Kuroda, Shigeyasu
Shimao, Ichiro
Morita, Noboru
Asao, Toyonobu
The regioselective synthesis of dimethyl 1,3,5-cycloheptariene-1,2-dicarboxylate (4) was achieved by a ring expansion method, starting from dimethyl 1,3-cyclohexadiene-2,3-dicarboxylate (5).The title compound 3 was obtained as an air-sensitive oil by zinc-copper reduction of 1,2-bis(bromomethyl)cyclohepta-1,3,5-triene (10) to which the diester 4 was transformed.
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