Bull. Russ. Acad. Sci. Div. Chem. Sci. (Engl. Transl.) p. 178 - 180 (1992)
Update date:2022-08-25
Topics:
Lapidus, A. L.
Pirozhkov, S. D.
Tumanova, A. R.
Koksharova, T. G.
Volkova, N. V.
et al.
A new method has been developed for the synthesis of the ethyl ester of the mononitrile of malonic acid by the carbonylation of benzenesulfonyloxyacetonitrile in absolute ethanol in the presence of cobalt carbonyl.The yield of the desired product was 30 percent with 60-90percent conversion of the starting compound.The effects of temperature, pressure, and reaction time was studied. Keywords: carbonylation, dicobalt octacarbonyl, benzenesulfonyloxyacetonitrile, ethyl ester of the mononitrile of malonic acid.
View MoreGUANGZHOU MEDCAN PHARMATECH LTD
website:http://www.gzmedcan.com
Contact:+86-20-82519649
Address:Building J,Room 101,1 JiangtashanRd,Guang Zhou Science City,Guang Zhou ,China
Refine Chemicals Science & Technology Technology Developing Co., Ltd.
Contact:+86-22-87899130
Address:No.12,west keyan road,Tianjin City
Contact:+44 (0)2036089360-31
Address:Chanceryhouse,Chancery Lan
Guangzhou Probig Fine Chemical Co., Ltd.
Contact:020-86297874
Address:No.2, 1/F, No.20, Hetai Road,Hebian Village, Baiyun District,Guangzhou,China
Xian Changyue Biological Technology Co., Ltd.
website:https://www.xachangyue.com/
Contact:+86-029-62886900
Address:Keji Road NO.70
Doi:10.1002/cjoc.201900141
(2019)Doi:10.1039/c5cc04286k
(2015)Doi:10.1016/j.tet.2014.06.081
(2015)Doi:10.1016/j.tetlet.2014.10.061
(2014)Doi:10.1016/S0040-4039(00)01671-3
(1953)Doi:10.1002/jlcr.822
(2004)