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Cas Database |
| Name |
Methyl syringate |
EINECS | 429-050-5 |
| CAS No. | 884-35-5 | Density | 1.221 g/cm3 |
| PSA | 64.99000 | LogP | 1.19600 |
| Solubility | Soluble in alcohol, ether, slightly soluble in water | Melting Point |
103-107 °C |
| Formula | C10H12O5 | Boiling Point | 339.9 °C at 760 mmHg |
| Molecular Weight | 212.202 | Flash Point | 132.4 °C |
| Transport Information | N/A | Appearance | beige powder |
| Safety | 37/39-26 | Risk Codes | 36/37/38 |
| Molecular Structure |
|
Hazard Symbols |
 Xi
|
| Synonyms |
DeniLite II Assist;Methyl 3,5-dimethoxy-4-hydroxybenzoate;Methyl4-hydroxy-3,5-dimethoxybenzoate;NSC 16946;NSC 611398;Novoprime F 258;Syringicacid, methyl ester (6CI);4-Hydroxy-3,5-dimethoxybenzoic acid methyl ester; |
Article Data | 33 |
Methyl syringate Synthetic route
| Conditions | Yield |
|---|---|
| With sulfuric acid for 6h; Reflux; | 100% |
| With sulfuric acid for 3h; Reflux; | 96% |
| With thionyl chloride at 50℃; for 18h; | 96% |
| Conditions | Yield |
|---|---|
| With iodine; magnesium In diethyl ether; dichloromethane at 80℃; for 1h; | 100% |
| Stage #1: 3,4,5-trimethoxybenzoic acid methyl ester With aluminum (III) chloride In dichloromethane at 20℃; Stage #2: With hydrogenchloride; water In dichloromethane; chloroform | 98% |
| Stage #1: 3,4,5-trimethoxybenzoic acid methyl ester With aluminum (III) chloride In dichloromethane at 20℃; Stage #2: With hydrogenchloride In chloroform | 98% |
| Conditions | Yield |
|---|---|
| With thionyl chloride at 0℃; Reflux; | 95% |
- 27065-65-2
methyl 4-benzyloxy-3,5-dimethoxybenzoate
- 884-35-5
methyl syringate
| Conditions | Yield |
|---|---|
| With sodium tetrahydroborate; nickel(II) chloride hexahydrate In methanol at 0℃; | 90% |
| With palladium on activated charcoal; ethanol Hydrogenation; | |
| With hydrogen; palladium on activated charcoal |
| Conditions | Yield |
|---|---|
| With sodium tetrahydroborate; tetrakis(triphenylphosphine) palladium(0) In tetrahydrofuran for 2h; Ambient temperature; | 90% |
| With sodium tetrahydroborate; nickel(II) chloride hexahydrate In methanol at 0℃; | 88% |
| Conditions | Yield |
|---|---|
| With ethylene glycol at 120℃; for 1h; | A 10% B 78% |
- 186581-53-3, 908094-01-9
diazomethane
- 86450-76-2
6-O-syringyl-8-O-acetyl shanzhiside methyl ester
A
- 884-35-5
methyl syringate
B
- 64421-28-9
shanzhiside methyl ester
| Conditions | Yield |
|---|---|
| With sodium hydroxide 1.) methanol, room temperature, 4 d; Multistep reaction; |
| Conditions | Yield |
|---|---|
| With sodium hydroxide for 96h; Ambient temperature; |
- 130774-07-1
Methyl syringate 4-O-α-L-rhamnopyranoside
- 884-35-5
methyl syringate
| Conditions | Yield |
|---|---|
| With hydrogenchloride In 1,4-dioxane; water for 1h; Heating; | 15 mg |
- 86450-76-2
6-O-syringyl-8-O-acetyl shanzhiside methyl ester
A
- 884-35-5
methyl syringate
B
- 29836-27-9
shanzhiside
| Conditions | Yield |
|---|---|
| With sodium hydroxide In methanol Ambient temperature; |
Methyl syringate Chemical Properties
IUPAC Name: Methyl 4-hydroxy-3,5-dimethoxybenzoate
Synonyms of Benzoic acid,4-hydroxy-3,5-dimethoxy-, methyl ester (CAS NO.884-35-5): AI3-364 ; Methyl 3,5-dimethoxy-4-hydroxybenzoate ; Methyl-4-hydroxy-3,5-dimethoxybenzoate ; 3,5-Dimethoxy-4-hydroxybenzoic acid methyl ester ; Rarechem al bf 0102;methyl syringoate ; Syringic acid monomethyl ester ; 4-Hydroxy-3,5-Dimethoxybenzoic Acid Methyl Ester
CAS NO: 884-35-5
Molecular Formula: C10H12O5
Molecular Weight: 212.1993
Molecular Structure:
.png)
Melting Point: 103-107 °C
Product Categories: Aromatic Esters ; Acids & Esters ; Anisoles, Alkyloxy Compounds & Phenylacetates ; Phenols ; Pharmaceutical Intermediate
H bond acceptors: 5
H bond donors: 1
Freely Rotating Bonds: 5
Polar Surface Area: 53.99 Å2
Index of Refraction: 1.525
Molar Refractivity: 53.26 cm3
Molar Volume: 173.7 cm3
Surface Tension: 41.2 dyne/cm
Density of Benzoic acid,4-hydroxy-3,5-dimethoxy-, methyl ester (CAS NO.884-35-5): 1.221 g/cm3
Flash Point: 132.4 °C
Enthalpy of Vaporization: 60.65 kJ/mol
Boiling Point: 339.9 °C at 760 mmHg
Vapour Pressure: 4.54E-05 mmHg at 25°C
Methyl syringate Safety Profile
Hazard Codes of Benzoic acid,4-hydroxy-3,5-dimethoxy-, methyl ester (CAS NO.884-35-5): 
Xi
Risk Statements: 36/37/38
R36/37/38: Irritating to eyes, respiratory system and skin.
Safety Statements: 37/39-26
S37/39: Wear suitable gloves and eye/face protection.
S26: In case of contact with eyes, rinse immediately with plenty of water and seek medical advice.
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