Technology Process of 3-(Trimethylstannyl)propan-1-ol
There total 4 articles about 3-(Trimethylstannyl)propan-1-ol which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
lithium;
In
tetrahydrofuran;
N2 atmosphere; addn. of the oxetane to a soln. of trimethylstannyllithium prepared from chlorotrimethylstannane and lithium at -78°C, stirring for 6 h at room temp.;; addn. of diethyl ether, washing with satd. NH4Cl soln., drying with Na2SO4, evapn. of the solvent, fractional distn.;
- Guidance literature:
-
In
not given;
refluxing for 5 h;;
- Guidance literature:
-
With
potassium hydroxide;
In
ethanol; water;
