Methyl 2-Fluoro-5-Methylbenzoate

Base Information

• Chemical Name: Methyl 2-Fluoro-5-Methylbenzoate
• CAS No.: 2967-93-3
• Molecular Formula: C9H9FO2
• Molecular Weight: 168.168
• Hs Code.: 2916399090
• Mol file: 2967-93-3.mol

Synonyms:Benzoic acid,2-fluoro-5-methyl-,methyl ester;2-fluoro-5-methyl-benzoic acid methyl ester;

Chemical Property of Methyl 2-Fluoro-5-Methylbenzoate

Chemical Property:

• PSA: 26.30000
• LogP: 1.92070
• Storage Temp.: Sealed in dry,Room Temperature

Purity/Quality:

97% ^*data from raw suppliers

Methyl2-fluoro-5-methylbenzoate ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Methyl 2-Fluoro-5-Methylbenzoate

There total 6 articles about Methyl 2-Fluoro-5-Methylbenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.3%

methanol (67-56-1) + 2-fluoro-5-methyl-benzoic acid (321-12-0) → 2-fluoro-5-methyl benzoic acid methyl ester (2967-93-3)

Guidance literature:

With thionyl chloride; for 3h; Reflux;

DOI:10.1039/c8ob00286j

Reference yield: 98.0%

→ 2-fluoro-5-methyl benzoic acid methyl ester (2967-93-3)

Guidance literature:

Reference yield: 94.0%

2-fluoro-5-methyl-benzoic acid (321-12-0) + dimethyl sulfate (77-78-1) → 2-fluoro-5-methyl benzoic acid methyl ester (2967-93-3)

Guidance literature:

With potassium carbonate; In acetone; Heating;

DOI:10.1016/S0968-0896(02)00153-0

upstream raw materials:

methanol

2-fluoro-5-methyl-benzoic acid

dimethyl sulfate

2-fluoro-5-methylbenzonitrile

Downstream raw materials:

2-fluoro-5-bromomethyl benzoic acid methyl ester

methyl 2-fluoro-5-formylbenzoate

C₂₁H₂₁FN₂O₄

1-(3-(4-(cyclopropylcarbonyl)piperazine-1-carbonyl)-4-fluorobenzyl)quinazoline-2,4(1H,3H)-dione

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