Carbamic acid, [5-(4-amino-3,5-dimethylphenoxy)-2-nitrophenyl]methyl-, 1,1-dimethylethyl ester

Base Information

• Chemical Name: Carbamic acid, [5-(4-amino-3,5-dimethylphenoxy)-2-nitrophenyl]methyl-, 1,1-dimethylethyl ester
• CAS No.: 223133-30-0
• Molecular Formula: C20H25N3O5
• Molecular Weight: 387.436

Synonyms:4-(4-amino-3,5,dimethylphenoxy)-2-(N-t-butoxycarbonyl-N-methylamino)nitrobenzene;N-(5-(4-amino-3,5-dimethylphenoxy)-2-nitrophenyl)-N-methylcarbamic acid t-butyl ester;t-butyl N-[5-(4-amino-3,5-dimethylphenoxy)-2-nitrophenyl]-N-methylcarbamate;2-(N-t-Butoxycarbonyl-N-methylamino)-4-(4-amino-3,5-dimethylphenoxy)nitrobenzene;t-Butyl N-[5-(4amino-3,5-dimethylphenoxy)-2-nitrophenyl]-N-methylcarbamate;

Chemical Property of Carbamic acid, [5-(4-amino-3,5-dimethylphenoxy)-2-nitrophenyl]methyl-, 1,1-dimethylethyl ester

Chemical Property:

• PSA: 110.61000
• LogP: 6.06180

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Carbamic acid, [5-(4-amino-3,5-dimethylphenoxy)-2-nitrophenyl]methyl-, 1,1-dimethylethyl ester

There total 3 articles about Carbamic acid, [5-(4-amino-3,5-dimethylphenoxy)-2-nitrophenyl]methyl-, 1,1-dimethylethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N-(2-nitro-5-chlorophenyl)-N-methylcarbamic acid t-butyl ester (299176-17-3) + 3,5-dimethyl-4-aminophenol (3096-70-6) → 2-(N-t-butoxycarbonyl-N-methylamino)-4-(4-amino-3,5-dimethylphenoxy)nitrobenzene (223133-30-0)

Guidance literature:

With sodium hydride; In DMF (N,N-dimethyl-formamide); at 120 ℃; for 1h;

Reference yield:

3,5-dimethyl-4-aminophenol (3096-70-6) + ethyl acetate (141-78-6) → 2-(N-t-butoxycarbonyl-N-methylamino)-4-(4-amino-3,5-dimethylphenoxy)nitrobenzene (223133-30-0)

Guidance literature:

In N-(2-nitro-5-chlorophenyl)-N-methylcarbamic acid t-butyl ester; hexane; N,N-dimethyl-formamide; mineral oil;

Reference yield:

→ 2-(N-t-butoxycarbonyl-N-methylamino)-4-(4-amino-3,5-dimethylphenoxy)nitrobenzene (223133-30-0)

Guidance literature:

upstream raw materials:

N-(2-nitro-5-chlorophenyl)-N-methylcarbamic acid t-butyl ester

3,5-dimethyl-4-aminophenol

ethyl acetate

Downstream raw materials:

4-{N-[2,6-dimethyl-4-(3-(N-t-butoxycarbonyl-N-methylamino)-4-nitrophenoxy)phenyl]aminomethyl}-2-propyl-1-[2'-(1-triphenylmethyl-1H-tetrazol-5-yl)biphenyl-4-ylmethyl]-1H-imidazole-5-carboxylic acid ethyl ester

tert-butyl (4-{[2-(hydroxymethyl)-1-methyl-1H-benzimidazol-6-yl]oxy}-2,6-dimethylphenyl)carbamate

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