4-(3,5-di-t-butyl-4-hydroxyphenylthio)-2-(N-t-butoxycarbonyl-N-methylamino)nitrobenzene

Base Information

• Chemical Name: 4-(3,5-di-t-butyl-4-hydroxyphenylthio)-2-(N-t-butoxycarbonyl-N-methylamino)nitrobenzene
• CAS No.: 223133-29-7
• Molecular Formula: C₂₆H₃₆N₂O₅S
• Molecular Weight: 488.648

Synonyms:4-(3,5-di-t-butyl-4-hydroxyphenylthio)-2-(N-t-butoxycarbonyl-N-methylamino)nitrobenzene

Chemical Property of 4-(3,5-di-t-butyl-4-hydroxyphenylthio)-2-(N-t-butoxycarbonyl-N-methylamino)nitrobenzene

Chemical Property:

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Technology Process of 4-(3,5-di-t-butyl-4-hydroxyphenylthio)-2-(N-t-butoxycarbonyl-N-methylamino)nitrobenzene

There total 1 articles about 4-(3,5-di-t-butyl-4-hydroxyphenylthio)-2-(N-t-butoxycarbonyl-N-methylamino)nitrobenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N-(2-nitro-5-chlorophenyl)-N-methylcarbamic acid t-butyl ester (299176-17-3) + 4-hydroxy-3,5-di-tert-butylthiophenol (950-59-4) → 4-(3,5-di-t-butyl-4-hydroxyphenylthio)-2-(N-t-butoxycarbonyl-N-methylamino)nitrobenzene (223133-29-7)

Guidance literature:

With potassium carbonate; In DMF (N,N-dimethyl-formamide); at 80 ℃; for 1h;

Reference yield:

4-(3,5-di-t-butyl-4-hydroxyphenylthio)-2-(N-t-butoxycarbonyl-N-methylamino)nitrobenzene (223133-29-7) + diethyl cyanophosphonate (2942-58-7) + [4-[[2,4-dioxo-1,3-thiazolidine-5-yl]methyl]phenoxy]acetic acid (179087-93-5) → t-butyl N-{2-[4-(2,4-dioxothiazolidin-5-ylmethyl)phenoxyacetylamino]-5-(3,5-di-t-butyl-4-hydroxyphenylthio)phenyl}-N-methylcarbamate

Guidance literature:

With triethylamine; palladium; In tetrahydrofuran; methanol; water;

Reference yield:

4-(3,5-di-t-butyl-4-hydroxyphenylthio)-2-(N-t-butoxycarbonyl-N-methylamino)nitrobenzene (223133-29-7) → 4-(3,5-di-t-butyl-4-hydroxyphenylthio)-2-(N-t-butoxycarbonyl-N-methylamino)aniline (299175-85-2)

Guidance literature:

palladium; In methanol;

upstream raw materials:

N-(2-nitro-5-chlorophenyl)-N-methylcarbamic acid t-butyl ester

4-hydroxy-3,5-di-tert-butylthiophenol

Downstream raw materials:

4-(3,5-di-t-butyl-4-hydroxyphenylthio)-2-(N-t-butoxycarbonyl-N-methylamino)aniline

5-{4-[6-(3,5-di-t-butyl-4-hydroxyphenylthio)-1-methyl-1H-benzimidazol-2-ylmethoxy]benzyl}thiazolidine-2,4-dione

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