1-(2-ETHYL-PHENYL)-1H-PYRROLE

Base Information

• Chemical Name: 1-(2-ETHYL-PHENYL)-1H-PYRROLE
• CAS No.: 299426-84-9
• Molecular Formula: C12H13N
• Molecular Weight: 171.242
• Hs Code.: 2933998090
• Mol file: 299426-84-9.mol

Synonyms:1-(2-ethylphenyl)pyrrole;1-(2-Ethyl-phenyl)-1H-pyrrole;

Chemical Property of 1-(2-ETHYL-PHENYL)-1H-PYRROLE

Chemical Property:

• PSA: 4.93000
• LogP: 3.03970

Purity/Quality:

99%, ^*data from raw suppliers

1-(2-Ethylphenyl)-1H-pyrrole 95% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

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Technology Process of 1-(2-ETHYL-PHENYL)-1H-PYRROLE

There total 2 articles about 1-(2-ETHYL-PHENYL)-1H-PYRROLE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

cis,trans-2,5-dimethoxytetrahydrofuran (696-59-3) + ortho-ethylaniline (578-54-1) → 1-(2-ethylphenyl)-1H-pyrrole (299426-84-9)

Guidance literature:

With nanosulfated titania; In neat (no solvent); at 120 ℃; for 0.416667h;

DOI:10.1007/s10593-014-1425-3

Reference yield: 30.0%

1,4-butenediol (6117-80-2) + ortho-ethylaniline (578-54-1) → 1-(2-ethylphenyl)-1H-pyrrole (299426-84-9)

Guidance literature:

With [2,2]bipyridinyl; sodium carbonate; nickel dichloride; In toluene; at 130 ℃; for 36h; Inert atmosphere; Schlenk technique;

DOI:10.1021/acs.joc.8b02666

Reference yield: 90.0%

1-(2-ethylphenyl)-1H-pyrrole (299426-84-9) → 2,5-dibromo-1-(2-ethylphenyl)-1H-pyrrole

Guidance literature:

With N-Bromosuccinimide; In N,N-dimethyl-formamide; at 0 ℃;

DOI:10.1016/j.tet.2016.07.032

upstream raw materials:

cis,trans-2,5-dimethoxytetrahydrofuran

ortho-ethylaniline

1,4-butenediol

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