3-Bromo-N-methyl-N-nitroso benzenemethanamine

Base Information

Chemical Name:3-Bromo-N-methyl-N-nitroso benzenemethanamine
CAS No.:98736-47-1
Molecular Formula:C₈H₉BrN₂O
Molecular Weight:229.076
Hs Code.:
UNII:US77V3W4HF
DSSTox Substance ID:DTXSID40879393
Nikkaji Number:J1.546.015F
Wikidata:Q27291238
ChEMBL ID:CHEMBL139530

Synonyms:m-Bromo-N-methyl-N-nitrosobenzylamine;3-Bromo-N-methyl-N-nitroso benzenemethanamine;98736-47-1;US77V3W4HF;NIOSH/DP1745000;N-Nitroso-N-(m-bromobenzyl)methylamine;N-Nitroso-N-(3-bromobenzyl)methylamine;Benzylamine, m-bromo-N-methyl-N-nitroso-;DP17450000;Benzenemethanamine, 3-bromo-N-methyl-N-nitroso-;CCRIS 2565;UNII-US77V3W4HF;CHEMBL139530;DTXSID40879393;Q27291238

Suppliers and Price of 3-Bromo-N-methyl-N-nitroso benzenemethanamine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-Bromo-N-methyl-N-nitroso benzenemethanamine

Chemical Property:

Vapor Pressure:4.37E-05mmHg at 25°C
Boiling Point:361.2°C at 760 mmHg
Flash Point:172.3°C
Density:1.45g/cm³
XLogP3:2.3
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:2
Exact Mass:227.98983
Heavy Atom Count:12
Complexity:154

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CN(CC1=CC(=CC=C1)Br)N=O

Technology Process of 3-Bromo-N-methyl-N-nitroso benzenemethanamine

There total 2 articles about 3-Bromo-N-methyl-N-nitroso benzenemethanamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 67344-77-8
1-(3-bromophenyl)-N-methylmethanamine

: 98736-47-1
N-nitroso-N-(3-bromobenzyl)methylamine

Guidance literature:: With hydrogenchloride; sodium nitrite; In water; acetic acid; Ambient temperature;
DOI:10.1021/jm00151a006

Reference yield:

: 823-78-9
meta-bromobenzyl bromide

: 98736-47-1
N-nitroso-N-(3-bromobenzyl)methylamine

Guidance literature:: Multi-step reaction with 2 steps

1: 87 percent / ethanol / 6 h / Heating

2: 82 percent / NaNO₂, aq. HCl / acetic acid; H₂O / Ambient temperature

With hydrogenchloride; sodium nitrite; In ethanol; water; acetic acid;
DOI:10.1021/jm00151a006