n-(1h-Benzotriazol-1-ylmethyl)-n-phenylaniline

Base Information

• Chemical Name: n-(1h-Benzotriazol-1-ylmethyl)-n-phenylaniline
• CAS No.: 15497-48-0
• Molecular Formula: C19H16 N4
• Molecular Weight: 300.3571
• NSC Number: 138163
• DSSTox Substance ID: DTXSID70300660
• Nikkaji Number: J545.273B
• Wikidata: Q82043912
• Mol file: 15497-48-0.mol

Synonyms:15497-48-0;N-(1H-1,2,3-Benzotriazol-1-ylmethyl)-N-phenylaniline;N-((1H-Benzo[d][1,2,3]triazol-1-yl)methyl)-N-phenylaniline;n-(1h-benzotriazol-1-ylmethyl)-n-phenylaniline;NSC138163;starbld0020174;CBDivE_009847;SCHEMBL7933277;DTXSID70300660;NSC-138163;(1H-1,2,3-Benzotriazol-1-ylmethyl)diphenylamine

Chemical Property of n-(1h-Benzotriazol-1-ylmethyl)-n-phenylaniline

Chemical Property:

• Vapor Pressure: 4.38E-10mmHg at 25°C
• Boiling Point: 498.8°C at 760 mmHg
• Flash Point: 255.5°C
• Density: 1.17g/cm³
• XLogP3: 4.7
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 3
• Rotatable Bond Count: 4
• Exact Mass: 300.137496527
• Heavy Atom Count: 23
• Complexity: 344

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1=CC=C(C=C1)N(CN2C3=CC=CC=C3N=N2)C4=CC=CC=C4

Technology Process of n-(1h-Benzotriazol-1-ylmethyl)-n-phenylaniline

There total 3 articles about n-(1h-Benzotriazol-1-ylmethyl)-n-phenylaniline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

1,2,3-Benzotriazole (95-14-7,27556-51-0) + formaldehyd (50-00-0,30525-89-4,61233-19-0) + diphenylamine (122-39-4) → benzotriazol-1-ylmethyl-diphenyl-amine (15497-48-0)

Guidance literature:

In methanol; for 4h; Cooling with ice;

DOI:10.4067/S0717-97072010000300021

Reference yield:

1-Hydroxymethyl-1H-benzotriazole (28539-02-8) + diphenylamine (122-39-4) → benzotriazol-1-ylmethyl-diphenyl-amine (15497-48-0)

Guidance literature:

DOI:10.1016/S0040-4039(00)92139-7

Reference yield:

→ benzotriazol-1-ylmethyl-diphenyl-amine (15497-48-0)

Guidance literature:

upstream raw materials:

1-Hydroxymethyl-1H-benzotriazole

diphenylamine

1,2,3-Benzotriazole

formaldehyd

Downstream raw materials:

But-3-enyl-diphenyl-amine

N,N-diphenylethylamine

N-phenyl-N-(2-phenylethyl)aniline

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