Technology Process of Bismuth, pentaphenyl-
There total 12 articles about Bismuth, pentaphenyl- which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
water;
In
cyclohexane; water;
byproducts: benzene; addn. of LiBiPh6 to water/ice/cyclohexane (stirring); benzene found in org. phase, collection of ppt. (filtn.), washing (ether), drying (vacuum);
- Guidance literature:
-
With
LiC6H5;
In
diethyl ether;
byproducts: LiCl; dropwise addn. of LiPh in stoich. amt., abs. diethyl ether, N2 atm., -75°C; washing with water, ethanol, ether, recrystn. from ethanol;
- Guidance literature:
-
With
LiC6H5;
In
diethyl ether;
molar ratio of ((C6H5)4Bi)Cl and phenyl lithium = 1:1.25, -70°C;