copper(I) carbonyl tris(3-phenylpyrazolyl)phosphine oxidehexafluorophosphate

Base Information

• Chemical Name: copper(I) carbonyl tris(3-phenylpyrazolyl)phosphine oxidehexafluorophosphate
• CAS No.: 1367554-43-5
• Molecular Formula: C₂₈H₂₁CuN₆O₂P*F₆P
• Molecular Weight: 712.998
• Mol file: 1367554-43-5.mol

Synonyms:

Chemical Property of copper(I) carbonyl tris(3-phenylpyrazolyl)phosphine oxidehexafluorophosphate

Chemical Property:

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Useful:

Technology Process of copper(I) carbonyl tris(3-phenylpyrazolyl)phosphine oxidehexafluorophosphate

There total 1 articles about copper(I) carbonyl tris(3-phenylpyrazolyl)phosphine oxidehexafluorophosphate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

carbon monoxide (201230-82-2) + copper(I) acetonitrile tris(3-phenylpyrazolyl)phosphine oxide hexafluorophosphate (1367554-22-0) → copper(I) carbonyl tris(3-phenylpyrazolyl)phosphine oxidehexafluorophosphate (1367554-43-5)

Guidance literature:

In dichloromethane; under N2; soln. of Cu complex in degassed CH2Cl2 degassed by three freeze-pump-thaw cycles; filled with CO (1 atm) before third thawing; after thawing, stirred at room temp. overnight; pentane added; solvent removed using cannula filter; solid dried under N2; mixt. of initial and resultant Cu complexes obtained; detd. by (1)H NMR spectra;

DOI:10.1021/om300051f

upstream raw materials:

carbon monoxide

copper(I) acetonitrile tris(3-phenylpyrazolyl)phosphine oxide hexafluorophosphate