2-(Bromomethyl)anthracene

Base Information

Chemical Name:2-(Bromomethyl)anthracene
CAS No.:31124-71-7
Molecular Formula:C15H11Br
Molecular Weight:271.156
Hs Code.:
DSSTox Substance ID:DTXSID80597382
Nikkaji Number:J1.757.143E
Wikidata:Q82492918
Mol file:31124-71-7.mol

Synonyms:2-(Bromomethyl)anthracene;31124-71-7;2-bromomethylanthracene;7-bromomethylanthracene;SCHEMBL5681757;DTXSID80597382;XAMMUQHFUJWZQX-UHFFFAOYSA-N;A936646

Suppliers and Price of 2-(Bromomethyl)anthracene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 0 raw suppliers

Chemical Property of 2-(Bromomethyl)anthracene

Chemical Property:

Boiling Point:411.7±14.0 °C(Predicted)
PSA：0.00000
Density:1.448±0.06 g/cm3(Predicted)
LogP:4.88790
XLogP3:4.9
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:0
Rotatable Bond Count:1
Exact Mass:270.00441
Heavy Atom Count:16
Complexity:238

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC=C2C=C3C=C(C=CC3=CC2=C1)CBr

Technology Process of 2-(Bromomethyl)anthracene

There total 1 articles about 2-(Bromomethyl)anthracene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 84-54-8
2-methylanthracene-9,10-dione

: 31124-71-7
2-(bromomethyl)anthracene

Guidance literature:: Multi-step reaction with 4 steps

1: zinc; ammonia; copper(ll) sulfate pentahydrate / 48 h / 80 °C

2: selenium(IV) oxide / 5,5-dimethyl-1,3-cyclohexadiene / 48 h / 130 °C

3: sodium tetrahydroborate / ethanol / Reflux

4: phosphorus tribromide / toluene / 0 - 5 °C

With selenium(IV) oxide; sodium tetrahydroborate; copper(ll) sulfate pentahydrate; ammonia; phosphorus tribromide; zinc; In 5,5-dimethyl-1,3-cyclohexadiene; ethanol; toluene;
DOI:10.1002/chem.202002648

Reference yield: 93.0%

: 31124-71-7
2-(bromomethyl)anthracene

: 603-35-0
triphenylphosphine

: 88229-63-4
(2-Anthrylmethyl)triphenylphosphonium Bromide

Guidance literature:: In xylene; at 100 ℃; for 24h;
DOI:10.1246/bcsj.67.3030

Reference yield:

: 31124-71-7
2-(bromomethyl)anthracene

: 78405-79-5
trans-1-(2-anthryl)-2-phenylethene

Guidance literature:: Multi-step reaction with 2 steps

1: 93 percent / xylene / 24 h / 100 °C

2: 0.8 g / sodium ethoxide / ethanol / 1.) 15 h, 2.) reflux, 3 h

With sodium ethanolate; In ethanol; xylene;
DOI:10.1246/bcsj.67.3030