2H-Pyrrolium, 5-ethyl-3,4-dihydro-1,2-dimethyl-4,4-diphenyl-,perchlorate

Base Information

Chemical Name:2H-Pyrrolium, 5-ethyl-3,4-dihydro-1,2-dimethyl-4,4-diphenyl-,perchlorate
CAS No.:31161-17-8
Deprecated CAS:105774-68-3
Molecular Formula:C20H24N.ClO4
Molecular Weight:
Hs Code.:
European Community (EC) Number:853-152-2
DSSTox Substance ID:DTXSID80880948
Mol file:31161-17-8.mol

Synonyms:31161-17-8;EDDP (perchlorate) (CRM);5-ethyl-1,2-dimethyl-4,4-diphenyl-2,3-dihydropyrrol-1-ium;perchlorate;d,l-EDDP.perchlorate;EDDP Perchlorate;2-Ethyl-1,5-dimethyl-3,3-diphenylpyrrolinium Perchlorate;5-Ethyl-3,4-dihydro-1,2-dimethyl-4,4-diphenyl-2H-pyrrolium perchlorate (1:1);SCHEMBL4902337;DTXSID80880948;d,l-EDDP.perchlorate, 1mg/ml in Methanol;EDDP Perchlorate (2-Ethyl-1,5-dimethyl-3,3-diphenylpyrrolinium Perchlorate);EDDP Perchlorate (2-Ethyl-1,5-dimethyl-3,3-diphenylpyrrolinium Perchlorate) 0.1 mg/ml in Methanol (as Pyrrolinium);EDDP Perchlorate (2-Ethyl-1,5-dimethyl-3,3-diphenylpyrrolinium Perchlorate) 1.0 mg/ml in Methanol (as Pyrrolinium)

Suppliers and Price of 2H-Pyrrolium, 5-ethyl-3,4-dihydro-1,2-dimethyl-4,4-diphenyl-,perchlorate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 2 raw suppliers

Chemical Property of 2H-Pyrrolium, 5-ethyl-3,4-dihydro-1,2-dimethyl-4,4-diphenyl-,perchlorate

Chemical Property:

Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:3
Exact Mass:377.1393859
Heavy Atom Count:26
Complexity:461

Purity/Quality:: 98%,99%, ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CCC1=[N+](C(CC1(C2=CC=CC=C2)C3=CC=CC=C3)C)C.[O-]Cl(=O)(=O)=O

Technology Process of 2H-Pyrrolium, 5-ethyl-3,4-dihydro-1,2-dimethyl-4,4-diphenyl-,perchlorate

There total 8 articles about 2H-Pyrrolium, 5-ethyl-3,4-dihydro-1,2-dimethyl-4,4-diphenyl-,perchlorate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 7576-08-1
(S)-(+)-2,2-diphenyl-4-dimethylaminopentanenitrile

: 31161-17-8
(S)-(-)-2-ethyl-1,5-dimethyl-3,3-diphenylpyrrolinium perchlorate

Guidance literature:: Multi-step reaction with 4 steps

1: NaHCO₃ / CHCl₃ / 48 h / Heating

2: conc. HCl / 42 h / Heating

3: 76 percent / 1.2 N HCl, NaNO₂ / 1 h / heating on a steam bath

4: 2.) 60percent HClO₄ / 1.) toluene, benzene, diethyl ether, room temperature

With hydrogenchloride; perchloric acid; sodium hydrogencarbonate; sodium nitrite; In chloroform;
DOI:10.1002/jhet.5570230212

Reference yield:

: 7576-16-1
(R)-(-)-2,2-diphenyl-4-dimethylaminopentanenitrile

: 31161-17-8
(R)-(+)-2-ethyl-1,5-dimethyl-3,3-diphenylpyrrolinium perchlorate

Guidance literature:: Multi-step reaction with 4 steps

1: NaHCO₃ / CHCl₃ / 48 h / Heating

2: conc. HCl / 42 h / Heating

3: 87 percent / 1.2 N HCl, NaNO₂ / 1 h / heating on a steam bath

4: 2.) 60percent HClO₄ / 1.) toluene, benzene, diethyl ether, room temperature

With hydrogenchloride; perchloric acid; sodium hydrogencarbonate; sodium nitrite; In chloroform;
DOI:10.1002/jhet.5570230212

Reference yield:

: 106293-51-0
(S)-(+)-2-imino-1,5-dimethyl-3,3-diphenylpyrrolidine

: 31161-17-8
(S)-(-)-2-ethyl-1,5-dimethyl-3,3-diphenylpyrrolinium perchlorate

Guidance literature:: Multi-step reaction with 2 steps

1: 76 percent / 1.2 N HCl, NaNO₂ / 1 h / heating on a steam bath

2: 2.) 60percent HClO₄ / 1.) toluene, benzene, diethyl ether, room temperature

With hydrogenchloride; perchloric acid; sodium nitrite;
DOI:10.1002/jhet.5570230212