(Z)-3-Chloro-2-methyl-3-phenyl-acrylaldehyde

Base Information

Chemical Name:(Z)-3-Chloro-2-methyl-3-phenyl-acrylaldehyde
CAS No.:31357-81-0
Molecular Formula:C10H9ClO
Molecular Weight:180.634
Hs Code.:2913000090
Mol file:31357-81-0.mol

Synonyms:(Z)-3-chloro-2-methyl-3-phenylacrylaldehyde;(Z)-3-chloro-2-methyl-3-(2-thyenyl)acrolein;(Z)-3-CHLORO-2-METHYL-3-(2-THENYL) ACROLEIN;(2Z)-3-chloro-2-methyl-3-(2-thienyl)acrylaldehyde;

Suppliers and Price of (Z)-3-Chloro-2-methyl-3-phenyl-acrylaldehyde

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
(Z)-3-CHLORO-2-METHYL-3-PHENYL-ACRYLALDEHYDE 95.00%
5MG
$ 501.97

Total 7 raw suppliers

Chemical Property of (Z)-3-Chloro-2-methyl-3-phenyl-acrylaldehyde

Chemical Property:

Boiling Point:100-105 °C(Press: 0.65 Torr)
PSA：17.07000
Density:1.137±0.06 g/cm3(Predicted)
LogP:2.85530

Purity/Quality:

95% ^*data from raw suppliers

(Z)-3-CHLORO-2-METHYL-3-PHENYL-ACRYLALDEHYDE 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of (Z)-3-Chloro-2-methyl-3-phenyl-acrylaldehyde

There total 3 articles about (Z)-3-Chloro-2-methyl-3-phenyl-acrylaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 68-12-2,33513-42-7
N,N-dimethyl-formamide

: 93-55-0
1-phenyl-propan-1-one

: 31357-81-0
(Z)-β-chloro-α-methyl-β-phenylacrolein

: 31357-82-1
(E)-β-chloro-α-methyl-β-phenylacrolein

Guidance literature:: With trichlorophosphate; at 60 - 70 ℃; for 6h; Yield given. Yields of byproduct given;
DOI:10.1080/00397919508015433

Reference yield:

: 68-12-2,33513-42-7
N,N-dimethyl-formamide

: 93-55-0
1-phenyl-propan-1-one

: 31357-81-0
(Z)-β-chloro-α-methyl-β-phenylacrolein

Guidance literature:: N,N-dimethyl-formamide; With trichlorophosphate; for 0.5h; Cooling with ice;

1-phenyl-propan-1-one; at 0 - 65 ℃; for 9h;
DOI:10.1021/acs.joc.6b01781