3-mesityl-5-(p-methoxyphenyl)isoxazol-4-yl(phenyl)iodonium toluene-p-sulphonate

Base Information

• Chemical Name: 3-mesityl-5-(p-methoxyphenyl)isoxazol-4-yl(phenyl)iodonium toluene-p-sulphonate
• CAS No.: 123466-34-2
• Molecular Formula: C₇H₇O₃S*C₂₅H₂₃INO₂
• Molecular Weight: 667.564
• Mol file: 123466-34-2.mol

Synonyms:

Chemical Property of 3-mesityl-5-(p-methoxyphenyl)isoxazol-4-yl(phenyl)iodonium toluene-p-sulphonate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 3-mesityl-5-(p-methoxyphenyl)isoxazol-4-yl(phenyl)iodonium toluene-p-sulphonate

There total 3 articles about 3-mesityl-5-(p-methoxyphenyl)isoxazol-4-yl(phenyl)iodonium toluene-p-sulphonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

[hydroxy(tosyloxy)iodo]benzene (27126-76-7) → 3-mesityl-5-(p-methoxyphenyl)isoxazol-4-yl(phenyl)iodonium toluene-p-sulphonate (123466-34-2)

Guidance literature:

Multi-step reaction with 2 steps

1: 35 percent / 20 h

2: CH₂Cl₂ / 48 h / Ambient temperature

In dichloromethane;

DOI:10.1039/P19890000827

Reference yield:

4-methoxyphenylacetylen (768-60-5) → 3-mesityl-5-(p-methoxyphenyl)isoxazol-4-yl(phenyl)iodonium toluene-p-sulphonate (123466-34-2)

Guidance literature:

Multi-step reaction with 2 steps

1: 35 percent / 20 h

2: CH₂Cl₂ / 48 h / Ambient temperature

In dichloromethane;

DOI:10.1039/P19890000827

Reference yield:

[(4-methoxyphenyl)ethynyl](phenyl)iodonium tosylate (123466-30-8) + mesitylenecarbonitrile oxide (2904-57-6) → 3-mesityl-5-(p-methoxyphenyl)isoxazol-4-yl(phenyl)iodonium toluene-p-sulphonate (123466-34-2) + 3-mesityl-4-(p-methoxyphenyl)isoxazol-5-yl(phenyl)iodonium toluene-p-sulphonate (123466-36-4)

Guidance literature:

In dichloromethane; for 48h; Title compound not separated from byproducts; Ambient temperature;

DOI:10.1039/P19890000827

upstream raw materials:

[(4-methoxyphenyl)ethynyl](phenyl)iodonium tosylate

mesitylenecarbonitrile oxide

[hydroxy(tosyloxy)iodo]benzene

4-methoxyphenylacetylen