1,1-Dimethylethyl (2Z)-3-(3-quinolinyl)-2-propen-1-yl carbonate

Base Information

Chemical Name:1,1-Dimethylethyl (2Z)-3-(3-quinolinyl)-2-propen-1-yl carbonate
CAS No.:314050-19-6
Molecular Formula:C17H19NO3
Molecular Weight:
Hs Code.:
European Community (EC) Number:608-617-2
DSSTox Substance ID:DTXSID101175518
Mol file:314050-19-6.mol

Synonyms:SCHEMBL372483;DTXSID101175518;1,1-Dimethylethyl (2Z)-3-(3-quinolinyl)-2-propen-1-yl carbonate;314050-19-6

Suppliers and Price of 1,1-Dimethylethyl (2Z)-3-(3-quinolinyl)-2-propen-1-yl carbonate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1,1-Dimethylethyl (2Z)-3-(3-quinolinyl)-2-propen-1-yl carbonate

Chemical Property:

Vapor Pressure:0mmHg at 25°C
XLogP3:3.9
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:6
Exact Mass:285.13649347
Heavy Atom Count:21
Complexity:373

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CC(C)(C)OC(=O)OCC=CC1=CC2=CC=CC=C2N=C1
Isomeric SMILES:CC(C)(C)OC(=O)OC/C=C\C1=CC2=CC=CC=C2N=C1

Technology Process of 1,1-Dimethylethyl (2Z)-3-(3-quinolinyl)-2-propen-1-yl carbonate

There total 2 articles about 1,1-Dimethylethyl (2Z)-3-(3-quinolinyl)-2-propen-1-yl carbonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 24424-99-5
di-tert-butyl dicarbonate

: 314050-18-5
cis-3-(3-quinolyl)-2-propen-1-ol

: 314050-19-6
cis-(3-(3-quinolyl)-2-propenyl) t-butyl carbonate

Guidance literature:: With sodium hydroxide; n-Bu₄HSO₄; In dichloromethane; at 0 ℃;
DOI:10.1021/jo034883z

Reference yield:

: 70437-05-7
3-(3-quinolinyl)-2-propyn-1-ol

: 314050-19-6
cis-(3-(3-quinolyl)-2-propenyl) t-butyl carbonate

Guidance literature:: Multi-step reaction with 2 steps

1: 50.0 g / H₂; 3,6-dithia-1,8-octanediol / Pd/CaCO₃-Pb / ethanol / 25 h / 19 °C / 15.51 Torr

2: 88 percent / n-Bu₄HSO₄; aq. NaOH / CH₂Cl₂ / 0 °C

With sodium hydroxide; 2,2'-ethane-1,2-diylbissulfanyl-bis-ethanol; n-Bu₄HSO₄; hydrogen; Lindlar's catalyst; In ethanol; dichloromethane;
DOI:10.1021/jo034883z