5H-1,3-Dithiolo[4,5-c]pyrrole, 2-[4-[[2-[2-[4-[bis[4-(1,1-dimethylethyl)phenyl](4-ethylphenyl)methyl]phen oxy]ethoxy]ethyl]thio]-5-(methylthio)-1,3-dithiol-2-ylidene]-

Base Information

Chemical Name:5H-1,3-Dithiolo[4,5-c]pyrrole, 2-[4-[[2-[2-[4-[bis[4-(1,1-dimethylethyl)phenyl](4-ethylphenyl)methyl]phen oxy]ethoxy]ethyl]thio]-5-(methylthio)-1,3-dithiol-2-ylidene]-
CAS No.:314286-46-9
Molecular Formula:C48H53NO2S6
Molecular Weight:868.35
Hs Code.:

5H-1,3-Dithiolo[4,5-c]pyrrole,
2-[4-[[2-[2-[4-[bis[4-(1,1-dimethylethyl)phenyl](4-ethylphenyl)methyl]phen
oxy]ethoxy]ethyl]thio]-5-(methylthio)-1,3-dithiol-2-ylidene]-

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Chemical Property of 5H-1,3-Dithiolo[4,5-c]pyrrole, 2-[4-[[2-[2-[4-[bis[4-(1,1-dimethylethyl)phenyl](4-ethylphenyl)methyl]phen oxy]ethoxy]ethyl]thio]-5-(methylthio)-1,3-dithiol-2-ylidene]-

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Technology Process of 5H-1,3-Dithiolo[4,5-c]pyrrole, 2-[4-[[2-[2-[4-[bis[4-(1,1-dimethylethyl)phenyl](4-ethylphenyl)methyl]phen oxy]ethoxy]ethyl]thio]-5-(methylthio)-1,3-dithiol-2-ylidene]-

There total 14 articles about 5H-1,3-Dithiolo[4,5-c]pyrrole, 2-[4-[[2-[2-[4-[bis[4-(1,1-dimethylethyl)phenyl](4-ethylphenyl)methyl]phen oxy]ethoxy]ethyl]thio]-5-(methylthio)-1,3-dithiol-2-ylidene]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 314286-45-8
2-{4-[2-(2-{4-[bis-(4-tert-butyl-phenyl)-(4-ethyl-phenyl)-methyl]-phenoxy}-ethoxy)-ethylsulfanyl]-5-methylsulfanyl-[1,3]dithiol-2-ylidene}-5-(toluene-4-sulfonyl)-5H-[1,3]dithiolo[4,5-c]pyrrole

: 314286-46-9
2-{4-[2-(2-{4-[bis-(4-tert-butyl-phenyl)-(4-ethyl-phenyl)-methyl]-phenoxy}-ethoxy)-ethylsulfanyl]-5-methylsulfanyl-[1,3]dithiol-2-ylidene}-5H-[1,3]dithiolo[4,5-c]pyrrole

Guidance literature:: With sodium methylate; In tetrahydrofuran; methanol; for 0.333333h; Heating;
DOI:10.1021/ol006387s

Reference yield:

: 177609-52-8
2-(2-{4-[bis(4-tert-butylphenyl)-(4-ethylphenyl)methyl]phenoxy}ethoxy)ethanol

: 314286-46-9
2-{4-[2-(2-{4-[bis-(4-tert-butyl-phenyl)-(4-ethyl-phenyl)-methyl]-phenoxy}-ethoxy)-ethylsulfanyl]-5-methylsulfanyl-[1,3]dithiol-2-ylidene}-5H-[1,3]dithiolo[4,5-c]pyrrole

Guidance literature:: Multi-step reaction with 4 steps

1: 53 percent / NaOH / tetrahydrofuran; H₂O / 4 h / 0 °C

2: 99 percent / NaI / acetone / 14 h / Heating

3: 1.32 g / tetrahydrofuran; methanol / 20 h / 20 °C

4: 92 percent / NaOMe / tetrahydrofuran; methanol / 0.33 h / Heating

With sodium hydroxide; sodium methylate; sodium iodide; In tetrahydrofuran; methanol; water; acetone;
DOI:10.1021/ja0114456

Reference yield:

: 177609-49-3
bis(4-tert-butylphenyl)(4-ethylphenyl)(4-hydroxyphenyl)methane

: 314286-46-9
2-{4-[2-(2-{4-[bis-(4-tert-butyl-phenyl)-(4-ethyl-phenyl)-methyl]-phenoxy}-ethoxy)-ethylsulfanyl]-5-methylsulfanyl-[1,3]dithiol-2-ylidene}-5H-[1,3]dithiolo[4,5-c]pyrrole

Guidance literature:: Multi-step reaction with 6 steps

1: KOH; LiBr / butan-1-ol / 60 h / Heating

2: 9.90 g / aq. HCl / methanol; CH₂Cl₂ / 2.5 h / 20 °C

3: 53 percent / NaOH / tetrahydrofuran; H₂O / 4 h / 0 °C

4: 99 percent / NaI / acetone / 14 h / Heating

5: 1.32 g / tetrahydrofuran; methanol / 20 h / 20 °C

6: 92 percent / NaOMe / tetrahydrofuran; methanol / 0.33 h / Heating

With hydrogenchloride; potassium hydroxide; sodium hydroxide; sodium methylate; sodium iodide; lithium bromide; In tetrahydrofuran; methanol; dichloromethane; water; acetone; butan-1-ol;
DOI:10.1021/ja0114456