Germane, trimethyl(3-methylphenyl)-

Base Information

Chemical Name:Germane, trimethyl(3-methylphenyl)-
CAS No.:31608-52-3
Molecular Formula:C10H16Ge
Molecular Weight:208.827
Hs Code.:
Mol file:31608-52-3.mol

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Germane, trimethyl(3-methylphenyl)-

Chemical Property:

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Safty Information:

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Hazard Codes:

MSDS Files:: SDS file from LookChem

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Technology Process of Germane, trimethyl(3-methylphenyl)-

There total 2 articles about Germane, trimethyl(3-methylphenyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 108-41-8
1-chloro-3-methylbenzene

: 429-41-4
tetrabutyl ammonium fluoride

: 31608-80-7
(trimethylsilyl)trimethylgermane

: 31608-52-3
m-MeC₆H₄GeMe₃

Guidance literature:: With water; In N,N,N,N,N,N-hexamethylphosphoric triamide; byproducts: PhMe; equimolar amts.; addn. of Bu4NF to Ge-compd., stirring at room temp. for5 min, addn. of org. halide, stirring at room temp. for 24 h, water add n.; extn. of org. layer (ether), drying, concn. (vac.), gas chromy. (yield 4.9%) and TLC;
DOI:10.1016/0022-328X(95)00315-H

Reference yield:

: 34557-54-5,27936-85-2
methane

: 865-52-1
tetramethylgermane

: 108-88-3,15644-74-3,16713-13-6
toluene

: 31608-52-3
m-MeC₆H₄GeMe₃

: 31608-53-4
trimethyl(4-methylphenyl)germane

Guidance literature:: With triethylamine; In gas; other Radiation; γ-irradiation (0.5-1E4 Gy/h, 600 Torr CH4, 20 Torr Me4Ge); in presence of 10 Torr O2; extn. into cyclohexane, gas chromy.; product ratio depending on educt ratio and amt. of Et3N;
DOI:10.1016/S0022-328X(97)00318-5

Reference yield: 85.0%

: 31608-52-3
m-MeC₆H₄GeMe₃

: 62-53-3
aniline

: 1205-64-7
3-Methyldiphenylamine

Guidance literature:: With sodium acetate; palladium diacetate; triphenylphosphine; In toluene; at 100 ℃; for 12h; Schlenk technique; Inert atmosphere;
DOI:10.1055/s-0035-1562104