4-tert-butylcyclohexyl phenyl ketone N,N-dimethylhydrazone

Base Information

• Chemical Name: 4-tert-butylcyclohexyl phenyl ketone N,N-dimethylhydrazone
• CAS No.: 1334580-17-4
• Molecular Formula: C₁₉H₃₀N₂
• Molecular Weight: 286.461
• Mol file: 1334580-17-4.mol

Synonyms:

Chemical Property of 4-tert-butylcyclohexyl phenyl ketone N,N-dimethylhydrazone

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 4-tert-butylcyclohexyl phenyl ketone N,N-dimethylhydrazone

There total 1 articles about 4-tert-butylcyclohexyl phenyl ketone N,N-dimethylhydrazone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

trans-1-Benzoyl-4-tert-butyl-cyclohexan (343623-01-8) + N,N-Dimethylhydrazine (57-14-7) → 4-tert-butylcyclohexyl phenyl ketone N,N-dimethylhydrazone (1334580-17-4)

Guidance literature:

With sodium acetate; acetic acid;

DOI:10.1002/chem.201101220

Reference yield:

4-tert-butylcyclohexyl phenyl ketone N,N-dimethylhydrazone (1334580-17-4) → cis-6-tert-butyl-2-phenyl-1-azaspiro[2,5]oct-1-ene + trans-6-tert-butyl-2-phenyl-1-azaspiro[2,5]oct-1-ene

Guidance literature:

Multi-step reaction with 2 steps

1: diethyl ether

2: sodium; isopropyl alcohol

With sodium; isopropyl alcohol; In diethyl ether;

DOI:10.1002/chem.201101220

Reference yield:

4-tert-butylcyclohexyl phenyl ketone N,N-dimethylhydrazone (1334580-17-4) + methyl iodide (74-88-4) → 4-tert-butylcyclohexyl phenyl ketone N,N,N-trimethylhydrazonium iodide (1334580-18-5)

Guidance literature:

In diethyl ether;

DOI:10.1002/chem.201101220

upstream raw materials:

trans-1-Benzoyl-4-tert-butyl-cyclohexan

N,N-Dimethylhydrazine

Downstream raw materials:

4-tert-butylcyclohexyl phenyl ketone N,N,N-trimethylhydrazonium iodide