2-(Allyloxy)benzyl BroMide

Base Information

Chemical Name:2-(Allyloxy)benzyl BroMide
CAS No.:319918-15-5
Molecular Formula:C10H11BrO
Molecular Weight:227.101
Hs Code.:
Mol file:319918-15-5.mol

Synonyms:2-allyloxy benzyl bromide;2-(Allyloxy)benzyl Bromide;

Suppliers and Price of 2-(Allyloxy)benzyl BroMide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
2-(Allyloxy)benzylBromide
50mg
$ 65.00

Crysdot
2-(Allyloxy)benzylBromide 95+%
5g
$ 751.00

Alichem
2-(Allyloxy)benzylBromide
5g
$ 826.10

AK Scientific
2-(Allyloxy)benzylBromide
5g
$ 1073.00

Total 5 raw suppliers

Chemical Property of 2-(Allyloxy)benzyl BroMide

Chemical Property:

Boiling Point:271.4±20.0 °C(Predicted)
PSA：9.23000
Density:1.327±0.06 g/cm3(Predicted)
LogP:3.14630

Purity/Quality:

97% ^*data from raw suppliers

2-(Allyloxy)benzylBromide ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 2-(Allyloxy)benzyl BroMide

There total 3 articles about 2-(Allyloxy)benzyl BroMide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 26906-01-4
2-allyloxybenzyl alcohol

: 319918-15-5
1-(bromomethyl)-2-(prop-2-en-1-yloxy)benzene

Guidance literature:: With t-butyl bromide; n-pentylmethylimidazolium bromide; for 1.1h; sonication;
DOI:10.1002/ejoc.200400597

Reference yield:

: 28752-82-1
2-(allyloxy)benzaldehyde

: 319918-15-5
1-(bromomethyl)-2-(prop-2-en-1-yloxy)benzene

Guidance literature:: Multi-step reaction with 2 steps

1: sodium tetrahydroborate / methanol / 0.17 h / 0 °C / Schlenk technique; Inert atmosphere

2: phosphorus tribromide / diethyl ether / 0 °C / Schlenk technique; Inert atmosphere

With sodium tetrahydroborate; phosphorus tribromide; In methanol; diethyl ether;
DOI:10.1021/acs.orglett.8b01857

Reference yield:

: 90-01-7
salicylic alcohol

: 319918-15-5
1-(bromomethyl)-2-(prop-2-en-1-yloxy)benzene

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate / acetone / 12 h / Reflux; Inert atmosphere

2: phosphorus tribromide / dichloromethane / 3 h / 0 - 20 °C / Inert atmosphere

With phosphorus tribromide; potassium carbonate; In dichloromethane; acetone;
DOI:10.1021/acs.jmedchem.8b00971