Cyclopropanol, 1-ethenyl-, 4-methylbenzenesulfonate

Base Information

Chemical Name:Cyclopropanol, 1-ethenyl-, 4-methylbenzenesulfonate
CAS No.:32364-41-3
Molecular Formula:C12H14O3S
Molecular Weight:238.307
Hs Code.:
Mol file:32364-41-3.mol

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Cyclopropanol, 1-ethenyl-, 4-methylbenzenesulfonate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

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Technology Process of Cyclopropanol, 1-ethenyl-, 4-methylbenzenesulfonate

There total 6 articles about Cyclopropanol, 1-ethenyl-, 4-methylbenzenesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 22935-31-5
1-Ethenylcyclopropan-1-ol

: 98-59-9
p-toluenesulfonyl chloride

: 32364-41-3
1-tosyloxy-1-vinylcyclopropane

Guidance literature:: With pyridine; at 0 ℃; for 14h;
DOI:10.1021/ja00037a006

Reference yield: 64.0%

: 13837-45-1
1-ethoxy-1-cyclopropanol

: 1826-67-1
vinyl magnesium bromide

: 98-59-9
p-toluenesulfonyl chloride

: 32364-41-3
1-tosyloxy-1-vinylcyclopropane

Guidance literature:: 1-ethoxy-1-cyclopropanol; vinyl magnesium bromide; In tetrahydrofuran; at 0 ℃; for 4h; Inert atmosphere; Reflux;

p-toluenesulfonyl chloride; In tetrahydrofuran; at 0 ℃; for 14h; Inert atmosphere;
DOI:10.1021/ol5015224

Reference yield:

: Toluene-4-sulfonic acid 1-ethynyl-cyclopropyl ester

: 32364-41-3
1-tosyloxy-1-vinylcyclopropane

Guidance literature:: With quinoline; hydrogen; Pd-BaSO₄; BaSO₄ deactivated with lead; In dichloromethane; for 24h; Yield given; Ambient temperature;