N-(2-cyclopropylidenethyl)-4-methyl-N-(2-methylallyl)benzenesulfonamide

Base Information

Chemical Name:N-(2-cyclopropylidenethyl)-4-methyl-N-(2-methylallyl)benzenesulfonamide
CAS No.:1063750-83-3
Molecular Formula:C₁₆H₂₁NO₂S
Molecular Weight:291.414
Hs Code.:

Synonyms:N-(2-cyclopropylidenethyl)-4-methyl-N-(2-methylallyl)benzenesulfonamide

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Chemical Property of N-(2-cyclopropylidenethyl)-4-methyl-N-(2-methylallyl)benzenesulfonamide

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Technology Process of N-(2-cyclopropylidenethyl)-4-methyl-N-(2-methylallyl)benzenesulfonamide

There total 1 articles about N-(2-cyclopropylidenethyl)-4-methyl-N-(2-methylallyl)benzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1206-41-3
N-(2-methylallyl)-4-toluenesulfonamide

: 32364-41-3
1-tosyloxy-1-vinylcyclopropane

: 1063750-83-3
N-(2-cyclopropylidenethyl)-4-methyl-N-(2-methylallyl)benzenesulfonamide

Guidance literature:: N-(2-methylallyl)-4-toluenesulfonamide; With sodium hydride; In N,N-dimethyl-formamide; mineral oil; at 20 ℃; for 1h; Inert atmosphere;

1-tosyloxy-1-vinylcyclopropane; With tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; 1,2-bis-(diphenylphosphino)ethane; In tetrahydrofuran; N,N-dimethyl-formamide; mineral oil; at 20 ℃; Inert atmosphere;

Reference yield: 91.0%

: 1063750-83-3
N-(2-cyclopropylidenethyl)-4-methyl-N-(2-methylallyl)benzenesulfonamide

: 1423-60-5
methyl ethynyl ketone

: 1-[(3aR*,8aS*)-8a-methyl-4-methylene-2-tosyl-1,2,3,3a,4,5,8,8a-octahydrocyclohepta[c]pyrrol-6-yl]ethanone

Guidance literature:: With triphenyl phosphite; chloro(1,5-cyclooctadiene)rhodium(I) dimer; In toluene; at 105 ℃; Inert atmosphere;

Reference yield: 81.0%

: 1063750-83-3
N-(2-cyclopropylidenethyl)-4-methyl-N-(2-methylallyl)benzenesulfonamide

: 201230-82-2
carbon monoxide

: 3a,7-dimethyl-2-tosyl-2,3,3a,4-tetrahydro-1H-isoindol-5(7aH)-one

Guidance literature:: With tris(triphenylphosphine)rhodium(I) chloride; silver trifluoroacetate; In para-xylene; at 120 ℃; for 12h; under 760.051 Torr; diastereoselective reaction; Schlenk technique;
DOI:10.1021/ja305467x