Benzene, 1-(1E)-1,3-butadienyl-4-methoxy-

Base Information

Chemical Name:Benzene, 1-(1E)-1,3-butadienyl-4-methoxy-
CAS No.:32507-39-4
Molecular Formula:C11H12O
Molecular Weight:160.216
Hs Code.:
Mol file:32507-39-4.mol

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Benzene, 1-(1E)-1,3-butadienyl-4-methoxy-

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

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Technology Process of Benzene, 1-(1E)-1,3-butadienyl-4-methoxy-

There total 45 articles about Benzene, 1-(1E)-1,3-butadienyl-4-methoxy- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 1963-36-6
4-methoxycinnamaldehyde

: 1779-49-3
Methyltriphenylphosphonium bromide

: 32507-39-4
(E)-1-(buta-1,3-diene-1-yl)-4-methoxybenzene

Guidance literature:: Methyltriphenylphosphonium bromide; With n-butyllithium; In tetrahydrofuran; hexane; at 0 ℃; for 0.5h; Inert atmosphere;

4-methoxycinnamaldehyde; In tetrahydrofuran; hexane; at 0 - 20 ℃; for 3h; Inert atmosphere;
DOI:10.1002/cjoc.201800205

Reference yield: 94.0%

: 24680-50-0,71277-11-7,1963-36-6
4-methoxy-trans-cinnamaldehyde

: 1779-49-3
Methyltriphenylphosphonium bromide

: 32507-39-4
(E)-1-(buta-1,3-diene-1-yl)-4-methoxybenzene

Guidance literature:: With potassium tert-butylate; In tetrahydrofuran; at 20 ℃; Inert atmosphere; Schlenk technique;
DOI:10.1021/acs.orglett.9b00531

Reference yield: 94.0%

: methylphosphonium bromide

: 24680-50-0,71277-11-7,1963-36-6
4-methoxy-trans-cinnamaldehyde

: 32507-39-4
(E)-1-(buta-1,3-diene-1-yl)-4-methoxybenzene

Guidance literature:: methylphosphonium bromide; With potassium tert-butylate; In tetrahydrofuran; at 20 ℃; for 0.5h; Inert atmosphere; Schlenk technique;

4-methoxy-trans-cinnamaldehyde; In tetrahydrofuran; at 20 ℃; for 16.1667h; Inert atmosphere; Schlenk technique;
DOI:10.1039/C8CC06153J