Technology Process of Stannane, dichlorobis(4-methylphenyl)-
There total 11 articles about Stannane, dichlorobis(4-methylphenyl)- which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
In
dichloromethane;
byproducts: bis(4-methylthiobenzoyl) disulfide; soln. of SnCl4 in CH2Cl2 added to soln. of piperidinium 4-methylbenzenecarbodithioate (molar ratio 1:4) in CH2Cl2; stirred at 20°C for 1h; solvent removed under reduced pressure; dissolved in CH2Cl2; filtered; sepd. by fractional crystn.; elem. anal.;
DOI:10.1016/S0022-328X(00)00453-8
- Guidance literature:
-
Multi-step reaction with 2 steps
1: Na-Sn alloy / xylene
2: HCl
With
Na-Sn alloy; HCl;
In
xylene;
- Guidance literature:
-
Multi-step reaction with 2 steps
1: Li; Sn-Hg alloy / diethyl ether
2: HCl
With
Li; Sn-Hg alloy; HCl;
In
diethyl ether;