3-Phenylnaphtho[1,2-b]furan

Base Information

• Chemical Name: 3-Phenylnaphtho[1,2-b]furan
• CAS No.: 32730-13-5
• Molecular Formula: C18H12O
• Molecular Weight: 244.293
• DSSTox Substance ID: DTXSID901310164
• Nikkaji Number: J1.217.870K
• Wikidata: Q107907106

Synonyms:3-Phenylnaphtho[1,2-b]furan;SCHEMBL11404213;DTXSID901310164;32730-13-5

Chemical Property of 3-Phenylnaphtho[1,2-b]furan

Chemical Property:

• XLogP3: 5.2
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 1
• Rotatable Bond Count: 1
• Exact Mass: 244.088815002
• Heavy Atom Count: 19
• Complexity: 307

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

• Canonical SMILES: C1=CC=C(C=C1)C2=COC3=C2C=CC4=CC=CC=C43

Technology Process of 3-Phenylnaphtho[1,2-b]furan

There total 10 articles about 3-Phenylnaphtho[1,2-b]furan which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

2-(naphthalen-1-yloxy)-1-phenylethanone (14621-59-1) → phenyl-3 naphto<1,2-b>furanne (32730-13-5)

Guidance literature:

With methanesulfonic acid; phosphorus pentoxide; at 45 ℃;

DOI:10.1177/1747519820907244

Reference yield: 91.0%

potassium; 3-hydroxy-3-phenyl-2,3-dihydro-naphtho[1,2-b]furan-2-carboxylate → phenyl-3 naphto<1,2-b>furanne (32730-13-5)

Guidance literature:

With hydrogenchloride; at 80 ℃; for 1h;

DOI:10.1016/j.tet.2004.11.022

Reference yield: 77.7%

α-naphthol (90-15-3) + α-bromoacetophenone (70-11-1) → 2-(naphthalen-1-yloxy)-1-phenylethanone (14621-59-1) + phenyl-3 naphto<1,2-b>furanne (32730-13-5)

Guidance literature:

With aluminum oxide; potassium carbonate; for 0.0833333h; Microwave irradiation;

DOI:10.1080/00397910902883702

upstream raw materials:

2-(naphthalen-1-yloxy)-1-phenylethanone

α-naphthyl benzoate

2-benzoyl-1-naphthol

(2-benzoyl-naphthalen-1-yloxy)-acetic acid ethyl ester

Downstream raw materials:

formyl-2 phenyl-3 naphto<1,2-b>furanne

acetyl-2 phenyl-3 naphto<1,2-b>furanne

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