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(CH3)3Sn(C6H8COOCH3)

Base Information
  • Chemical Name:(CH3)3Sn(C6H8COOCH3)
  • CAS No.:111076-03-0
  • Molecular Formula:C11H20O2Sn
  • Molecular Weight:302.989
  • Hs Code.:
(CH<sub>3</sub>)3Sn(C<sub>6</sub>H<sub>8</sub>COOCH<sub>3</sub>)

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Chemical Property of (CH3)3Sn(C6H8COOCH3)
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Technology Process of (CH3)3Sn(C6H8COOCH3)

There total 1 articles about (CH3)3Sn(C6H8COOCH3) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
In toluene; soln. 2-trimethylstannyl-1,3-butadiene and methyl acrylate in toluene refluxed overnight under nitrogen; solvent evapd., residue purified by column chromy. (eluent: ether/petroleum ether 1:20); elem. anal.;
Guidance literature:
In toluene; byproducts: Me3SnCl; soln. of PhSeCl added to soln. of mixt. of the two Sn compds.; resulting mixt. stirred overnight at room temp.; KF and THF added to destroy Me3SnCl; stirring at room temp. for 2 h; slurry filtered through short column of basic alumina; evapn. of solvent gave an oil consisting of mixt. of the two Se compds. (detd. 1H NMR spect. and by capillary gas-liquid chromy.);
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