1-[2-(2-Nitrophenyl)ethenyl]pyrrolidine

Base Information

• Chemical Name: 1-[2-(2-Nitrophenyl)ethenyl]pyrrolidine
• CAS No.: 32989-69-8
• Molecular Formula: C12H14N2O2
• Molecular Weight: 218.255
• DSSTox Substance ID: DTXSID60709769

Synonyms:2-nitro-beta-pyrrolidinostyrene;SCHEMBL8533307;DTXSID60709769;PUBVPFSOLOXTIV-UHFFFAOYSA-N;2-(2-pyrolidinylvinyl)nitrobenzene;1-[2-(2-NITROPHENYL)ETHENYL]PYRROLIDINE

Chemical Property of 1-[2-(2-Nitrophenyl)ethenyl]pyrrolidine

Chemical Property:

• Vapor Pressure: 0mmHg at 25°C
• XLogP3: 2.6
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 3
• Rotatable Bond Count: 2
• Exact Mass: 218.105527694
• Heavy Atom Count: 16
• Complexity: 267

Purity/Quality:

98% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1CCN(C1)C=CC2=CC=CC=C2[N+](=O)[O-]

Technology Process of 1-[2-(2-Nitrophenyl)ethenyl]pyrrolidine

There total 4 articles about 1-[2-(2-Nitrophenyl)ethenyl]pyrrolidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

pyrrolidine (123-75-1) + 1-methyl-2-nitrobenzene (88-72-2) + N,N-dimethyl-formamide dimethyl acetal (4637-24-5) → trans-2-nitro-β-pyrrolidinostyrene (32989-69-8)

Guidance literature:

In N,N-dimethyl-formamide; at 60 - 80 ℃; for 22h;

DOI:10.1016/S0040-4020(03)00973-6

Reference yield: 70.0%

pyrrolidine (123-75-1) + 1-methyl-2-nitrobenzene (88-72-2) + N,N-dimethylformamide diethyl diacetal (1188-33-6) → trans-2-nitro-β-pyrrolidinostyrene (32989-69-8)

Guidance literature:

In N,N-dimethyl-formamide; at 180 ℃; for 24h; Reflux; Inert atmosphere;

DOI:10.1134/S1070363219120363

Reference yield:

1-methyl-2-nitrobenzene (88-72-2) + 1-(dimethoxymethyl)pyrrolidine (5564-73-8) → trans-2-nitro-β-pyrrolidinostyrene (32989-69-8)

Guidance literature:

With nitrogen; In methanol; N,N-dimethyl-formamide;

upstream raw materials:

pyrrolidine

1-methyl-2-nitrobenzene

N,N-dimethyl-formamide dimethyl acetal

N,N-dimethylformamide diethyl diacetal

Downstream raw materials:

2-(2-nitrophenyl)acetaldehyde dimethyl acetal

indole

[1-(1-benzyl-piperidin-4-yl)-1H-indol-3-yl]-oxo-acetic acid methyl ester

oxo-[1-(1-pyridin-2-ylmethyl-piperidin-4-yl)-1H-indol-3-yl]-oxo-acetic acid methyl ester

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