4-tert-Butyl-4'-methoxy-2,3,4,5-tetrahydro-1,1'-biphenyl

Base Information

Chemical Name:4-tert-Butyl-4'-methoxy-2,3,4,5-tetrahydro-1,1'-biphenyl
CAS No.:33061-20-0
Molecular Formula:C17H24O
Molecular Weight:244.377
Hs Code.:
DSSTox Substance ID:DTXSID40526739
Nikkaji Number:J551.914D

Synonyms:33061-20-0;DTXSID40526739;4-tert-Butyl-4'-methoxy-2,3,4,5-tetrahydro-1,1'-biphenyl

Suppliers and Price of 4-tert-Butyl-4'-methoxy-2,3,4,5-tetrahydro-1,1'-biphenyl

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-tert-Butyl-4'-methoxy-2,3,4,5-tetrahydro-1,1'-biphenyl

Chemical Property:

XLogP3:5.1
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:3
Exact Mass:244.182715385
Heavy Atom Count:18
Complexity:289

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CC(C)(C)C1CCC(=CC1)C2=CC=C(C=C2)OC

Technology Process of 4-tert-Butyl-4'-methoxy-2,3,4,5-tetrahydro-1,1'-biphenyl

There total 7 articles about 4-tert-Butyl-4'-methoxy-2,3,4,5-tetrahydro-1,1'-biphenyl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 104-92-7
1-bromo-4-methoxy-benzene

: 98-53-3
4-tercbutyl-cyclohexanone

: 33061-20-0
1-(4-tert-butylcyclohex-1-en-1-yl)-4-methoxybenzene

Guidance literature:: 4-tercbutyl-cyclohexanone; With tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; toluene-4-sulfonic acid hydrazide; lithium tert-butoxide; XPhos; In 1,4-dioxane; for 0.0166667h; Inert atmosphere;

1-bromo-4-methoxy-benzene; In 1,4-dioxane; at 110 ℃; for 12h; Inert atmosphere;
DOI:10.1002/chem.200800390

Reference yield: 92.0%

: 13139-86-1
4-methoxyphenyl magnesium bromide

: 611235-47-3
toluene-4-sulfonic acid 4-tert-butylcyclohex-1-en-1-yl ester

: 33061-20-0
1-(4-tert-butylcyclohex-1-en-1-yl)-4-methoxybenzene

Guidance literature:: 4-methoxyphenyl magnesium bromide; With C₂₄H₅₂Cl₂O₁₂P₄Pd₂; In tetrahydrofuran; 1,4-dioxane; at 20 ℃; for 0.0833333h; Inert atmosphere;

toluene-4-sulfonic acid 4-tert-butylcyclohex-1-en-1-yl ester; In tetrahydrofuran; 1,4-dioxane; at 80 ℃; for 24h; Inert atmosphere;
DOI:10.1002/chem.201002386