3-Methoxy-4-[(2-nitrobenzyl)oxy]benzaldehyde

Base Information

Chemical Name:3-Methoxy-4-[(2-nitrobenzyl)oxy]benzaldehyde
CAS No.:331463-81-1
Molecular Formula:C15H13NO5
Molecular Weight:287.272
Hs Code.:2913000090
DSSTox Substance ID:DTXSID00355961
Wikidata:Q82135063
Mol file:331463-81-1.mol

Synonyms:3-methoxy-4-[(2-nitrobenzyl)oxy]benzaldehyde;331463-81-1;3-methoxy-4-[(2-nitrophenyl)methoxy]benzaldehyde;3-Methoxy-4-((2-nitrobenzyl)oxy)benzaldehyde;Oprea1_361323;Oprea1_790165;DTXSID00355961;MFCD00610825;STL291102;AKOS000194173;BS-37761;CS-0241461;FT-0725315;4-({2-nitrobenzyl}oxy)-3-methoxybenzaldehyde;EN300-232996;AG-690/09286059;Z26337697

Suppliers and Price of 3-Methoxy-4-[(2-nitrobenzyl)oxy]benzaldehyde

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Crysdot
3-Methoxy-4-((2-nitrobenzyl)oxy)benzaldehyde 95+%
10g
$ 947.00

Crysdot
3-Methoxy-4-((2-nitrobenzyl)oxy)benzaldehyde 95+%
5g
$ 569.00

ChemBridge Corporation
3-methoxy-4-[(2-nitrobenzyl)oxy]benzaldehyde 95%
1 g
$ 46.00

American Custom Chemicals Corporation
3-METHOXY-4-[(2-NITROBENZYL)OXY]BENZALDEHYDE 95.00%
5G
$ 1018.71

American Custom Chemicals Corporation
3-METHOXY-4-[(2-NITROBENZYL)OXY]BENZALDEHYDE 95.00%
1G
$ 685.21

Total 5 raw suppliers

Chemical Property of 3-Methoxy-4-[(2-nitrobenzyl)oxy]benzaldehyde

Chemical Property:

Vapor Pressure:1.5E-08mmHg at 25°C
Boiling Point:457.4oC at 760 mmHg
Flash Point:200.4oC
PSA：81.35000
Density:1.296g/cm3
LogP:3.51810
XLogP3:2.6
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:5
Rotatable Bond Count:5
Exact Mass:287.07937252
Heavy Atom Count:21
Complexity:357

Purity/Quality:

99% ^*data from raw suppliers

3-Methoxy-4-((2-nitrobenzyl)oxy)benzaldehyde 95+% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:COC1=C(C=CC(=C1)C=O)OCC2=CC=CC=C2[N+](=O)[O-]

Technology Process of 3-Methoxy-4-[(2-nitrobenzyl)oxy]benzaldehyde

There total 4 articles about 3-Methoxy-4-[(2-nitrobenzyl)oxy]benzaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 121-33-5,8014-42-4
vanillin

: 3958-60-9
2-nitrophenylmethyl bromide

: 331463-81-1
3-methoxy-4-(o-nitrobenzyloxy)benzaldehyde

Guidance literature:: With potassium carbonate; In acetone; Heating;
DOI:10.1021/jo052337v

Reference yield: 85.0%

: 3-hydroxy-4-(o-nitrobenzyloxy)benzaldehyde

: 74-88-4
methyl iodide

: 331463-81-1
3-methoxy-4-(o-nitrobenzyloxy)benzaldehyde

Guidance literature:: With sodium hydroxide; tetra(n-butyl)ammonium hydrogensulfate; In tetrahydrofuran; water; at 20 ℃; for 24h;
DOI:10.3390/70900697

Reference yield:

: 3958-60-9
2-nitrophenylmethyl bromide

: 331463-81-1
3-methoxy-4-(o-nitrobenzyloxy)benzaldehyde

Guidance literature:: Multi-step reaction with 2 steps

1: 67 percent / sodium iodide; sodium bicarbonate / dimethylformamide / 24 h / 40 °C

2: 85 percent / NaOH; Bu₄NHSO₄ / H₂O; tetrahydrofuran / 24 h / 20 °C

With sodium hydroxide; tetra(n-butyl)ammonium hydrogensulfate; sodium hydrogencarbonate; sodium iodide; In tetrahydrofuran; water; N,N-dimethyl-formamide;
DOI:10.3390/70900697