1,2-Bis(2-methoxyethoxy)-4,5-dinitrobenzene

Base Information

Chemical Name:1,2-Bis(2-methoxyethoxy)-4,5-dinitrobenzene
CAS No.:33332-63-7
Molecular Formula:C12H16N2O8
Molecular Weight:316.268
Hs Code.:
DSSTox Substance ID:DTXSID70530389
Wikidata:Q82401485

Synonyms:1,2-Bis(2-methoxyethoxy)-4,5-dinitrobenzene;33332-63-7;DTXSID70530389

Suppliers and Price of 1,2-Bis(2-methoxyethoxy)-4,5-dinitrobenzene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 2 raw suppliers

Chemical Property of 1,2-Bis(2-methoxyethoxy)-4,5-dinitrobenzene

Chemical Property:

XLogP3:1.2
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:8
Rotatable Bond Count:8
Exact Mass:316.09066547
Heavy Atom Count:22
Complexity:322

Purity/Quality:: 99%+, ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:COCCOC1=C(C=C(C(=C1)[N+](=O)[O-])[N+](=O)[O-])OCCOC

Technology Process of 1,2-Bis(2-methoxyethoxy)-4,5-dinitrobenzene

There total 4 articles about 1,2-Bis(2-methoxyethoxy)-4,5-dinitrobenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 17178-10-8,58320-73-3
2-methoxy-ethyl p-toluenesulfonyloxy ester

: 77400-30-7
1,2-dihydroxy-4,5-dinitrobenzene

: 33332-63-7
1,2-bis(2-methoxyethoxy)-4,5-dinitrobenzene

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; at 80 ℃; for 44h; Inert atmosphere;
DOI:10.1021/ja510585u

Reference yield: 41.0%

: 33332-53-5
3,4-bis-(2-methoxyethoxy)benzene

: 33332-63-7
1,2-bis(2-methoxyethoxy)-4,5-dinitrobenzene

Guidance literature:: With nitric acid; acetic acid; In dichloromethane; at 15 - 20 ℃; for 72h;
DOI:10.1002/anie.201306765

Reference yield:

: 120-80-9,19481-10-8,37349-32-9
benzene-1,2-diol

: 33332-63-7
1,2-bis(2-methoxyethoxy)-4,5-dinitrobenzene

Guidance literature:: Multi-step reaction with 3 steps

1: (i) Na, MeOCH₂CH₂OH, (ii) /BRN= 1731028/

2: (nitration)

3: NH₄NO₃, H₂SO₄ / acetic acid

With ammonium nitrate; sulfuric acid; In acetic acid;