3-Iodo-n,n-dimethylaniline

Base Information

Chemical Name:3-Iodo-n,n-dimethylaniline
CAS No.:33454-16-9
Molecular Formula:C8H10IN
Molecular Weight:247.079
Hs Code.:
DSSTox Substance ID:DTXSID70563137
Nikkaji Number:J2.342.016C
Wikidata:Q82447496

Synonyms:3-iodo-n,n-dimethylaniline;33454-16-9;Benzenamine, 3-iodo-N,N-dimethyl-;MFCD24133896;m-iodo-N,N-dimethylaniline;SCHEMBL1651699;DTXSID70563137;TVFNKBQQVHGWAF-UHFFFAOYSA-N;AKOS020189364;SY290789;G63615

Suppliers and Price of 3-Iodo-n,n-dimethylaniline

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 3 raw suppliers

Chemical Property of 3-Iodo-n,n-dimethylaniline

Chemical Property:

Boiling Point:215-216 °C(Press: 190 Torr)
PSA：3.24000
Density:1.652±0.06 g/cm3(Predicted)
LogP:2.35720
XLogP3:3.1
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:1
Exact Mass:246.98580
Heavy Atom Count:10
Complexity:103

Purity/Quality:: 99%, ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CN(C)C1=CC(=CC=C1)I

Technology Process of 3-Iodo-n,n-dimethylaniline

There total 12 articles about 3-Iodo-n,n-dimethylaniline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 121-69-7,77733-26-7
N,N-dimethyl-aniline

: 33454-16-9
3-iodo-N,N-dimethylaniline

Guidance literature:: N,N-dimethyl-aniline; With (TMEDA)Na(TMP)(t-Bu)Zn(t-Bu); In hexane; at 20 ℃; Inert atmosphere;

With iodine; Inert atmosphere;
DOI:10.3762/bjoc.7.144

Reference yield: 99.0%

: 16518-62-0
3-bromo-N,N-dimethylaniline

: 33454-16-9
3-iodo-N,N-dimethylaniline

Guidance literature:: With copper(l) iodide; sodium iodide; N,N`-dimethylethylenediamine; In 1,4-dioxane; N,N-dimethyl-formamide; at 110 ℃; for 22h; Inert atmosphere;
DOI:10.1002/anie.201711296