4-Iodo-N-[(E)-(4-nitrophenyl)methylidene]aniline

Base Information

Chemical Name:4-Iodo-N-[(E)-(4-nitrophenyl)methylidene]aniline
CAS No.:3382-81-8
Molecular Formula:C13H9IN2O2
Molecular Weight:352.12700
Hs Code.:
DSSTox Substance ID:DTXSID001245730
Nikkaji Number:J1.828.413H

Synonyms:N-(4-iodophenyl)-1-(4-nitrophenyl)methanimine;4-Iodo-N-[(E)-(4-nitrophenyl)methylidene]aniline;(4-iodophenyl)(4-nitrobenzylidene)amine;DTXSID001245730;STK035745;n-(4-nitrobenzylidene)-4-iodoaniline;4-iodo-N-(4-nitrobenzylidene)aniline;AKOS000485675;Benzene, 1-iodo-4-(4-nitrobenzylidenamino)-;4-Iodo-N-[(4-nitrophenyl)methylene]benzenamine;AE-848/00219049;4-Iodo-N-[(E)-(4-nitrophenyl)methylidene]aniline #;N-(4-iodophenyl)-N-[(E)-1-(4-nitrophenyl)methylidene]amine;3382-81-8

Suppliers and Price of 4-Iodo-N-[(E)-(4-nitrophenyl)methylidene]aniline

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 1 raw suppliers

Chemical Property of 4-Iodo-N-[(E)-(4-nitrophenyl)methylidene]aniline

Chemical Property:

PSA：58.18000
LogP:4.47320
XLogP3:3.7
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:2
Exact Mass:351.97088
Heavy Atom Count:18
Complexity:301

Purity/Quality:: 95% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:C1=CC(=CC=C1C=NC2=CC=C(C=C2)I)[N+](=O)[O-]

Technology Process of 4-Iodo-N-[(E)-(4-nitrophenyl)methylidene]aniline

There total 2 articles about 4-Iodo-N-[(E)-(4-nitrophenyl)methylidene]aniline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 555-16-8
4-nitrobenzaldehdye

: 540-37-4
p-aminoiodobenzene

: 3382-81-8,503027-98-3
4-iodo-N-(4-nitrobenzylidene)aniline

Guidance literature:: With molecular sieve; In ethanol; for 4h; Heating;
DOI:10.1248/cpb.55.1070

Reference yield:

: 3382-81-8,503027-98-3
4-iodo-N-(4-nitrobenzylidene)aniline

Guidance literature:: 4-Nitrobenzaldehyd, 4-Iodanilin;

Reference yield: 78.0%

: 3382-81-8,503027-98-3
4-iodo-N-(4-nitrobenzylidene)aniline

: 1600-27-7
mercury(II) diacetate

: 144271-75-0
2-(chloromercurio)-4-iodo-N-(4-nitrobenzylidene)aniline

Guidance literature:: With lithium chloride; In methanol; mixt. of Schiff base and Hg(OAc)2 (equal amts., concn. ca 0.1 M) in MeOH stirred and refluxed for 4 h, cooled to room temp.; addn. of LiCl soln.in hot MeOH; resulting thick mixt. stirred for about 10 min; ppt. filtered off, washed with ether, dried (vac.), crystn. from CHCl3; elem. anal.;
DOI:10.1021/om00059a058