2-Methyl-N-(2-phenylacetyl)alanine

Base Information

• Chemical Name: 2-Methyl-N-(2-phenylacetyl)alanine
• CAS No.: 34028-19-8
• Molecular Formula: C12H15NO3
• Molecular Weight: 221.25200
• Hs Code.: 2924299090

Synonyms:N-Phenylacetyl-p-nitroaniline;Phenylacetic acid p-nitroanilide;N-phenylacetyl-2-methylalanine;2-Methyl-2-(2-phenylacetamido)propionsaeure;N-Phenylacetyl-4-nitroaniline;4'-nitro(phenyl)acetanilide;

Chemical Property of 2-Methyl-N-(2-phenylacetyl)alanine

Chemical Property:

• PSA: 66.40000
• LogP: 1.59940

Purity/Quality:

98%min ^*data from raw suppliers

2-Methyl-N-(2-phenylacetyl)alanine ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2-Methyl-N-(2-phenylacetyl)alanine

There total 8 articles about 2-Methyl-N-(2-phenylacetyl)alanine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

N,N,2-Trimethyl-2-(2-phenylacetamido)propionamid (77919-02-9) → N-2-phenylacetyl-α-amino-2-methylpropionic acid (34028-19-8)

Guidance literature:

With hydrogenchloride; In water; acetonitrile;

DOI:10.1002/hlca.19870700112

Reference yield: 72.0%

N-phenylacetyl-N-(4-methoxybenzyl)-α,α-dimethylglycine cyclohexyl amide (658044-01-0) → N-2-phenylacetyl-α-amino-2-methylpropionic acid (34028-19-8)

Guidance literature:

With trifluoroacetic acid; for 0.166667h; Heating;

DOI:10.1039/b307111c

Reference yield: 67.2%

2-Aminoisobutyric acid (62-57-7) + phenylacetyl chloride (103-80-0) → N-2-phenylacetyl-α-amino-2-methylpropionic acid (34028-19-8)

Guidance literature:

With sodium hydroxide; for 2h;

DOI:10.1016/S0022-328X(01)01291-8

upstream raw materials:

2-Aminoisobutyric acid

phenylacetyl chloride

N,N,2-Trimethyl-2-(2-phenylacetamido)propionamid

2-methyl-2-phenylacetylamino-propionic acid tert-butyl ester

Downstream raw materials:

2-benzyl-4,4-dimethyl-4H-oxazol-5-one

2-methyl-2-phenylacetylamino-propionic acid methyl ester

2-Methyl-2-<2-methyl-2-(2-phenylacetamido)propionamido>propionsaeure

N-Isopropyl-2-methyl-2-<2-methyl-2-(2-phenylacetamido)propionamido>propionamid

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