N-phenylacetyl-N-(4-methoxybenzyl)-α,α-dimethylglycine cyclohexyl amide

Base Information

Chemical Name:N-phenylacetyl-N-(4-methoxybenzyl)-α,α-dimethylglycine cyclohexyl amide
CAS No.:658044-01-0
Molecular Formula:C₂₆H₃₄N₂O₃
Molecular Weight:422.568
Hs Code.:

Synonyms:N-phenylacetyl-N-(4-methoxybenzyl)-α,α-dimethylglycine cyclohexyl amide

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Chemical Property of N-phenylacetyl-N-(4-methoxybenzyl)-α,α-dimethylglycine cyclohexyl amide

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Technology Process of N-phenylacetyl-N-(4-methoxybenzyl)-α,α-dimethylglycine cyclohexyl amide

There total 3 articles about N-phenylacetyl-N-(4-methoxybenzyl)-α,α-dimethylglycine cyclohexyl amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 103-82-2
phenylacetic acid

: 931-53-3
Cyclohexyl isocyanide

: 2393-23-9
4-methoxy-benzylamine

: 67-64-1
acetone

: 658044-01-0
N-phenylacetyl-N-(4-methoxybenzyl)-α,α-dimethylglycine cyclohexyl amide

Guidance literature:: 4-methoxy-benzylamine; acetone; With sodium sulfate; for 0.25h;

phenylacetic acid; In methanol; for 0.25h;

Cyclohexyl isocyanide; In methanol; at 20 ℃;
DOI:10.1016/j.tet.2006.05.078

Reference yield:

: 2393-23-9
4-methoxy-benzylamine

: 658044-01-0
N-phenylacetyl-N-(4-methoxybenzyl)-α,α-dimethylglycine cyclohexyl amide

Guidance literature:: Multi-step reaction with 2 steps

1.1: Na₂SO₄ / 0.25 h / 20 °C

2.1: acetone / 0.17 h / 20 °C

2.2: 19.28 g / acetone / 20 °C

With sodium sulfate; In acetone;
DOI:10.1039/b307111c

Reference yield:

: 103-82-2
phenylacetic acid

: 931-53-3
Cyclohexyl isocyanide

: isopropylidene-(4-methoxy-benzyl)-amine

: 658044-01-0
N-phenylacetyl-N-(4-methoxybenzyl)-α,α-dimethylglycine cyclohexyl amide

Guidance literature:: phenylacetic acid; isopropylidene-(4-methoxy-benzyl)-amine; In acetone; at 20 ℃; for 0.166667h;

Cyclohexyl isocyanide; In acetone; at 20 ℃; Further stages.;
DOI:10.1039/b307111c