[(κ3-tris(1-phenyl-1H-1,2,3-triazol-4-yl)phosphine oxide)PtPh(η2-cis-2-butylene)]BF4

Base Information

Chemical Name:[(κ3-tris(1-phenyl-1H-1,2,3-triazol-4-yl)phosphine oxide)PtPh(η2-cis-2-butylene)]BF4
CAS No.:1354729-37-5
Molecular Formula:BF₄*C₃₄H₃₁N₉OPPt
Molecular Weight:894.538
Hs Code.:

Synonyms:

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Chemical Property of [(κ3-tris(1-phenyl-1H-1,2,3-triazol-4-yl)phosphine oxide)PtPh(η2-cis-2-butylene)]BF4

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Technology Process of [(κ3-tris(1-phenyl-1H-1,2,3-triazol-4-yl)phosphine oxide)PtPh(η2-cis-2-butylene)]BF4

There total 1 articles about [(κ3-tris(1-phenyl-1H-1,2,3-triazol-4-yl)phosphine oxide)PtPh(η2-cis-2-butylene)]BF4 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 67969-82-8
tetrafluoroboric acid diethyl ether

: 590-18-1
(Z)-2-Butene

: 1352287-04-7
diphenyl(κ2-tris(1-phenyl-1H-1,2,3-triazol-4-yl)phosphine oxide)platinum(II)

: 1354729-37-5
[(κ3-tris(1-phenyl-1H-1,2,3-triazol-4-yl)phosphine oxide)PtPh(η2-cis-2-butylene)]BF4

Guidance literature:: In dichloromethane; (N2); using Schlenk techniques; placing of Pt(C6H5)2(OP(C2HN3C6H5)2) in Schlenk flask, addn. of CH2Cl2 through septum, cooling to -78°C, treatment with 1 equiv. of HBF4*Et2O, warming to room temp., treatment with cis-butene; removal of solvent by rotary evapn., trituration with pentane;
DOI:10.1021/om2010595

Reference yield:

: 1354729-37-5
[(κ3-tris(1-phenyl-1H-1,2,3-triazol-4-yl)phosphine oxide)PtPh(η2-cis-2-butylene)]BF4

: [(κ3-tris(1-phenyl-1H-1,2,3-triazol-4-yl)phosphine oxide)PtH(CH(CH3)CH(CH3)-o-C6H4)]BF4

: [(κ3-tris(1-phenyl-1H-1,2,3-triazol-4-yl)phosphine oxide)PtH(CH(CH3)CH(CH3)-o-C6H4)]BF4

Guidance literature:: In chloroform-d1; (N2); using Schlenk techniques; addn. of CDCl3 to Pt(C6H5)(η2-cis-2-butylene)(OP(C2HN3C6H5)3)BF4 in NMR tube through septum, heating for 30 min at 50°C; removal of solvent by rotary evapn., trituration with pentane;
DOI:10.1021/om2010595