alpha-(4-Anilinophenylimino)-6-methoxy-O-cresol

Base Information

• Chemical Name: alpha-(4-Anilinophenylimino)-6-methoxy-O-cresol
• CAS No.: 6380-73-0
• Molecular Formula: C₂₀H₁₈N₂O₂
• Molecular Weight: 318.375
• European Community (EC) Number: 666-132-1

Synonyms:6380-73-0;2-{[(4-anilinophenyl)imino]methyl}-6-methoxyphenol;2-Methoxy-6-(((4-(phenylamino)phenyl)imino)methyl)phenol;Oprea1_106668;Oprea1_431757;CBDivE_010242;ALPHA-(4-ANILINOPHENYLIMINO)-6-METHOXY-O-CRESOL;AKOS003408079

Chemical Property of alpha-(4-Anilinophenylimino)-6-methoxy-O-cresol

Chemical Property:

• XLogP3: 4.4
• Hydrogen Bond Donor Count: 2
• Hydrogen Bond Acceptor Count: 4
• Rotatable Bond Count: 5
• Exact Mass: 318.136827821
• Heavy Atom Count: 24
• Complexity: 387

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

• Canonical SMILES: COC1=CC=CC(=C1O)C=NC2=CC=C(C=C2)NC3=CC=CC=C3

Technology Process of alpha-(4-Anilinophenylimino)-6-methoxy-O-cresol

There total 1 articles about alpha-(4-Anilinophenylimino)-6-methoxy-O-cresol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3-methoxy-2-hydroxybenzaldehyde (148-53-8) + N-phenylphenylene-1,4-diamine (101-54-2) → N-o-vanillidene-p-aminodiphenylamine (6380-73-0)

Guidance literature:

In ethanol; for 2h; Heating;

Reference yield:

N-o-vanillidene-p-aminodiphenylamine (6380-73-0) + antimonypentachloride (7647-18-9) → SbCl4(C6H5NHC6H4CHNOHC6H3OCH3)2(1+)*Cl(1-)=SbCl5(C6H5NHC6H4NCHOHC6H3OCH3)2 (92881-77-1)

Guidance literature:

In benzene; SbCl5 was mixed with ligand in benzene with shaking, mixt. was allowed to react overnight; filtered, washed with benzene, dried in vac. over P2O5; elem. anal.;

DOI:10.1016/S0020-1693(00)81868-X

Reference yield:

N-o-vanillidene-p-aminodiphenylamine (6380-73-0) + dimethylsilicon dichloride (75-78-5,30107-43-8) → 2-Methoxy-6-{[(E)-4-phenylamino-phenylimino]-methyl}-phenol; compound with dichloro-dimethyl-silane

Guidance literature:

In benzene;

upstream raw materials:

3-methoxy-2-hydroxybenzaldehyde

N-phenylphenylene-1,4-diamine

Downstream raw materials:

SbCl₄(C₆H₅NHC₆H₄CHNOHC₆H₃OCH₃)2⁽¹⁺⁾*Cl^(1-)=SbCl₅(C₆H₅NHC₆H₄NCHOHC₆H₃OCH₃)2

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