4-Fluorobenzaldehyde 2-phenylhydrazone

Base Information

Chemical Name:4-Fluorobenzaldehyde 2-phenylhydrazone
CAS No.:352-06-7
Molecular Formula:C13H11FN2
Molecular Weight:214.242
Hs Code.:
DSSTox Substance ID:DTXSID901285129
Mol file:352-06-7.mol

Synonyms:4-Fluorobenzaldehyde 2-phenylhydrazone;DTXSID901285129;352-06-7

Suppliers and Price of 4-Fluorobenzaldehyde 2-phenylhydrazone

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 1 raw suppliers

Chemical Property of 4-Fluorobenzaldehyde 2-phenylhydrazone

Chemical Property:

XLogP3:3.6
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:3
Exact Mass:214.09062652
Heavy Atom Count:16
Complexity:216

Purity/Quality:: 95% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC=C(C=C1)NN=CC2=CC=C(C=C2)F

Technology Process of 4-Fluorobenzaldehyde 2-phenylhydrazone

There total 4 articles about 4-Fluorobenzaldehyde 2-phenylhydrazone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 459-57-4
4-fluorobenzaldehyde

: 100-63-0
phenylhydrazine

: 352-06-7
1-(4-fluorobenzylidene)-2-phenylhydrazine

Guidance literature:: With oxaline; In neat (no solvent); at 25 - 30 ℃; for 0.00833333h; Green chemistry;
DOI:10.1016/j.molliq.2013.11.036

Reference yield: 84.0%

: phenyl hydrazine hydrochloride

: 459-57-4
4-fluorobenzaldehyde

: 352-06-7
1-(4-fluorobenzylidene)-2-phenylhydrazine

Guidance literature:: phenyl hydrazine hydrochloride; With sodium hydroxide;

4-fluorobenzaldehyde; With sulfuric acid; In ethanol;
DOI:10.1002/chem.202001590

Reference yield:

: 62-53-3
aniline

: 352-06-7
1-(4-fluorobenzylidene)-2-phenylhydrazine

Guidance literature:: Multi-step reaction with 2 steps

1.1: hydrogenchloride; sodium nitrite / water / 0.25 h / 0 °C

1.2: 0.5 h / 0 °C

2.1: sodium acetate / ethanol; water / 20 - 80 °C

With hydrogenchloride; sodium acetate; sodium nitrite; In ethanol; water;
DOI:10.1021/jo2005632