N-(3-chlorophenyl)-2-sulfanylacetamide

Base Information

Chemical Name:N-(3-chlorophenyl)-2-sulfanylacetamide
CAS No.:35331-31-8
Molecular Formula:C8H8ClNOS
Molecular Weight:201.677
Hs Code.:
DSSTox Substance ID:DTXSID00354772
Nikkaji Number:J1.060.726D
Wikidata:Q82133173
Mol file:35331-31-8.mol

Synonyms:N-(3-chlorophenyl)-2-sulfanylacetamide;35331-31-8;N-(3-Chlorophenyl)-2-mercaptoacetamide;SCHEMBL8288438;DTXSID00354772;HMS1674G18;N-(3-Chlorophenyl)mercaptoacetamide;MFCD00227541;AKOS000569890;MS-1412

Suppliers and Price of N-(3-chlorophenyl)-2-sulfanylacetamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 2 raw suppliers

Chemical Property of N-(3-chlorophenyl)-2-sulfanylacetamide

Chemical Property:

XLogP3:2.5
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:2
Exact Mass:201.0015127
Heavy Atom Count:12
Complexity:165

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC(=CC(=C1)Cl)NC(=O)CS

Technology Process of N-(3-chlorophenyl)-2-sulfanylacetamide

There total 5 articles about N-(3-chlorophenyl)-2-sulfanylacetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 2-S-(acetylthio)-N-(3’-chlorophenyl)acetamide

: 35331-31-8
N-(3-chlorophenyl)-2-mercaptoacetamide

Guidance literature:: With potassium hydroxide; In methanol; water; at 20 ℃; for 1.33h;
DOI:10.1039/d1md00187f

Reference yield: 97.0%

: 68-11-1
mercaptoacetic acid

: 108-42-9
3-chloro-aniline

: 35331-31-8
N-(3-chlorophenyl)-2-mercaptoacetamide

Guidance literature:: at 130 ℃; for 5h; Inert atmosphere;
DOI:10.1016/j.ejmech.2014.09.001

Reference yield:

: 108-42-9
3-chloro-aniline

: 35331-31-8
N-(3-chlorophenyl)-2-mercaptoacetamide

Guidance literature:: Multi-step reaction with 3 steps

1: N-ethyl-N,N-diisopropylamine; chloroacetyl chloride / dichloromethane / 4.33 h / 0 °C

2: potassium thioacetate / acetone / 3 h / 20 °C

3: potassium hydroxide / methanol; water / 1.33 h / 20 °C

With N-ethyl-N,N-diisopropylamine; chloroacetyl chloride; potassium hydroxide; potassium thioacetate; In methanol; dichloromethane; water; acetone;
DOI:10.1039/d1md00187f