Hexanenitrile, 2,2,5-trimethyl-

Base Information

• Chemical Name: Hexanenitrile, 2,2,5-trimethyl-
• CAS No.: 35863-42-4
• Molecular Formula: C9H17N
• Molecular Weight: 139.241
• Mol file: 35863-42-4.mol

Synonyms:

Chemical Property of Hexanenitrile, 2,2,5-trimethyl-

Chemical Property:

Purity/Quality:

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MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Hexanenitrile, 2,2,5-trimethyl-

There total 1 articles about Hexanenitrile, 2,2,5-trimethyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C10H17NO2 (134225-59-5) → 2,2,5-trimethylhex-4-enenitrile (13899-89-3) + 2,2,5-trimethyl-hexanenitrile (35863-42-4) + 2,2,5-Trimethyl-hex-5-enenitrile + 2,2,5-Trimethyl-5-(2,2,5,5-tetramethyl-cyclopentylideneamino)-hexanenitrile + 2,2,5,5-tetramethylcyclopentanone azine (89050-93-1) + C10H17NO2 (134225-59-5)

Guidance literature:

In acetonitrile; at 25 ℃; Product distribution; Mechanism; Irradiation; also photolysis in CCl₄;

Reference yield:

chloro-trimethyl-silane (75-77-4) + 2,2,5-trimethyl-hexanenitrile (35863-42-4) → 2,5-dimethylhexane (592-13-2) + Trimethyl-(trimethyl-1,1,4-pentyl)silan

Guidance literature:

With potassium; In N,N,N,N,N,N-hexamethylphosphoric triamide; diethyl ether; at 0 ℃;

Reference yield:

2,2,5-trimethyl-hexanenitrile (35863-42-4) → N-(4-cyano-2,2,5-trimethylhexyl)-4-methylbenzenesulfonamide + C17H26N2O2S

Guidance literature:

Multi-step reaction with 4 steps

1.1: lithium aluminium tetrahydride / tetrahydrofuran / 12 h / 0 - 25 °C / Schlenk technique; Inert atmosphere

2.1: triethylamine / dichloromethane / 0 - 25 °C

3.1: sodium hydride / dichloromethane / 25 °C / Schlenk technique; Inert atmosphere

3.2: 12 h / 25 °C / Schlenk technique; Inert atmosphere

4.1: Bathocuproine; copper(l) cyanide / 1,2-dichloro-ethane / 12 h / 60 °C / Schlenk technique; Inert atmosphere

With lithium aluminium tetrahydride; Bathocuproine; copper(l) cyanide; sodium hydride; triethylamine; In tetrahydrofuran; dichloromethane; 1,2-dichloro-ethane;

DOI:10.1021/acs.orglett.9b00553

upstream raw materials:

C₁₀H₁₇NO₂

Downstream raw materials:

2,5-dimethylhexane

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