N-(4-Methoxyphenyl)cyclohexanimine

Base Information

Chemical Name:N-(4-Methoxyphenyl)cyclohexanimine
CAS No.:36132-65-7
Molecular Formula:C13H17NO
Molecular Weight:203.284
Hs Code.:
DSSTox Substance ID:DTXSID20497498
Nikkaji Number:J1.081.334D
Mol file:36132-65-7.mol

Synonyms:N-(4-Methoxyphenyl)cyclohexanimine;36132-65-7;SCHEMBL8743958;DTXSID20497498

Suppliers and Price of N-(4-Methoxyphenyl)cyclohexanimine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemical Property of N-(4-Methoxyphenyl)cyclohexanimine

Chemical Property:

XLogP3:2.7
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:2
Exact Mass:203.131014166
Heavy Atom Count:15
Complexity:209

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:COC1=CC=C(C=C1)N=C2CCCCC2

Technology Process of N-(4-Methoxyphenyl)cyclohexanimine

There total 6 articles about N-(4-Methoxyphenyl)cyclohexanimine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 942046-57-3
cyclohexanone O-pentafluorobenzoyloxime

: 5720-07-0
4-methoxyphenylboronic acid

: 36132-65-7
N-(cyclohexylidene)-4-methoxyaniline

Guidance literature:: With 4 A molecular sieve; copper(I) thiophene-2-carboxylate; In N,N-dimethyl-formamide; at 50 ℃; for 2h;
DOI:10.1021/ol070561w

Reference yield: 82.0%

: 108-94-1,11119-77-0,9003-41-2,9075-99-4
cyclohexanone

: 104-94-9
4-methoxy-aniline

: 36132-65-7
N-(cyclohexylidene)-4-methoxyaniline

Guidance literature:: With acetic acid; In toluene; Heating;
DOI:10.1007/BF00531545

Reference yield:

: 100-64-1
cyclohexanone-oxime

: 36132-65-7
N-(cyclohexylidene)-4-methoxyaniline

Guidance literature:: Multi-step reaction with 2 steps

1: 93 percent / Et₃N / CH₂Cl₂ / 0.5 h / 0 °C

2: 82 percent / 4 Angstroem molecular sieves / Cu(I) thiophene-2-carboxylate / dimethylformamide / 2 h / 50 °C

With 4 A molecular sieve; triethylamine; copper(I) thiophene-2-carboxylate; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/ol070561w