6-METHOXY-2,2,4-TRIMETHYL-1,2-DIHYDROQUINOLINE

Base Information

• Chemical Name: 6-METHOXY-2,2,4-TRIMETHYL-1,2-DIHYDROQUINOLINE
• CAS No.: 4053-50-3
• Molecular Formula: C13H17NO
• Molecular Weight: 203.28
• Mol file: 4053-50-3.mol

Synonyms:

Chemical Property of 6-METHOXY-2,2,4-TRIMETHYL-1,2-DIHYDROQUINOLINE

Chemical Property:

Purity/Quality:

97% ^*data from raw suppliers

6-Methoxy-2,2,4-trimethyl-1,2-dihydro-quinoline 95 ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 6-METHOXY-2,2,4-TRIMETHYL-1,2-DIHYDROQUINOLINE

There total 3 articles about 6-METHOXY-2,2,4-TRIMETHYL-1,2-DIHYDROQUINOLINE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

4-methoxy-aniline (104-94-9) + acetone (67-64-1) → 6-methoxy-2,2,4-trimethyl-1,2-dihydro-quinoline (4053-50-3)

Guidance literature:

scandium tris(trifluoromethanesulfonate); at 20 ℃; for 2h;

DOI:10.1016/S0040-4039(02)00614-7

Reference yield: 28.0%

4-methyl-pent-3-en-2-one (141-79-7) + 4-methoxy-aniline (104-94-9) → 6-methoxy-2,2,4-trimethyl-1,2-dihydro-quinoline (4053-50-3)

Guidance literature:

With iodine; at 100 ℃; for 2h;

DOI:10.1021/jm049676l

Reference yield:

→ 6-methoxy-2,2,4-trimethyl-1,2-dihydro-quinoline (4053-50-3)

Guidance literature:

langsames Einleiten von Aceton unter die Oberflaeche einer 170-175grad heissen Schmelze von p-Anisidin in Ggw. von Jod;

upstream raw materials:

4-methoxy-aniline

acetone

4-methyl-pent-3-en-2-one

Downstream raw materials:

4,5-dihydro-4,4-dimethyl-8-methoxy-2,3-dithiolo<5,4c>quinoline-1-thione

1-(6-methoxy-4-methylquinazolin-2-yl)guanidine

1-acetyl-6-methoxy-4-phenyl-1,2,3,4-tetrahydro-2,2,4-trimethylquinoline

1-acetyl-6-hydroxy-4-phenyl-1,2,3,4-tetrahydro-2,2,4-trimethylquinoline

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