Morpholine, 4-(2-phenylethenyl)-

Base Information

• Chemical Name: Morpholine, 4-(2-phenylethenyl)-
• CAS No.: 36838-59-2
• Molecular Formula: C12H15NO
• Molecular Weight: 189.257
• Mol file: 36838-59-2.mol

Synonyms:2-morpholino-styrene;Morpholine,4-(2-phenylethenyl);4-(2-phenylethenyl) morpholine;1-morpholino-2-phenylethylene;4-styryl-morpholine;N-styrylmorpholine;

Chemical Property of Morpholine, 4-(2-phenylethenyl)-

Chemical Property:

• PSA: 12.47000
• LogP: 1.92740

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Morpholine, 4-(2-phenylethenyl)-

There total 19 articles about Morpholine, 4-(2-phenylethenyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

morpholine (110-91-8,99108-56-2) + phenylacetaldehyde (122-78-1) → N-styrylmorpholine (36838-59-2)

Guidance literature:

In benzene; Heating;

DOI:10.1055/s-1982-29947

Reference yield: 75.0%

4-(3-phenyl-prop-2-ynyl)-morpholine (1017-73-8) → 4-[(2Z)-3-phenylprop-2-en-1-yl]morpholine (63541-20-8,85620-81-1,85620-82-2,36838-59-2)

Guidance literature:

4-(3-phenyl-prop-2-ynyl)-morpholine; With niobium pentachloride; magnesium; In 1,2-dimethoxyethane; benzene; at 20 - 40 ℃; for 7h;

With potassium hydroxide; In 1,2-dimethoxyethane; diethyl ether; benzene; regioselective reaction; Cooling with ice;

DOI:10.3390/molecules26123722

Reference yield: 68.0%

erythro-2-diphenylphosphinoyl-3-morpholino-1-phenylpropan-1-ol (85620-74-2,85620-75-3,114893-64-0,114893-65-1) → 4-[(2Z)-3-phenylprop-2-en-1-yl]morpholine (63541-20-8,85620-81-1,85620-82-2,36838-59-2)

Guidance literature:

With sodium hydride; In N,N-dimethyl-formamide; at 30 ℃;

DOI:10.1016/S0040-4039(00)85639-7

upstream raw materials:

morpholine

2-oxo-3-(phenyl)propionic acid

phenylacetaldehyde

titanium(IV) isopropylate

Downstream raw materials:

4-(2,2-dimethoxy-1-phenyl-ethyl)-morpholine

4-(2,2-diethoxy-1-phenyl-ethyl)-morpholine

N,N-dimethyl-2-phenylethanethioamide

Dimethyl-dithiocarbamic acid 2-oxo-1-phenyl-ethyl ester