Benzene, [[(7-iodo-1-methylheptyl)oxy]methyl]-

Base Information

Chemical Name:Benzene, [[(7-iodo-1-methylheptyl)oxy]methyl]-
CAS No.:370863-08-4
Molecular Formula:C15H23IO
Molecular Weight:346.252
Hs Code.:
Mol file:370863-08-4.mol

Synonyms:

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Chemical Property of Benzene, [[(7-iodo-1-methylheptyl)oxy]methyl]-

Chemical Property:

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Technology Process of Benzene, [[(7-iodo-1-methylheptyl)oxy]methyl]-

There total 6 articles about Benzene, [[(7-iodo-1-methylheptyl)oxy]methyl]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 370863-07-3
7-benzyloxyoctanol

: 370863-08-4
7-benzyloxy-1-iodooctane

Guidance literature:: With 1H-imidazole; iodine; triphenylphosphine; In diethyl ether; at 0 ℃;

Reference yield:

: 13379-30-1
8-(tetrahydro-2H-pyran-2-yl)oxy-2-octanol

: 370863-08-4
7-benzyloxy-1-iodooctane

Guidance literature:: Multi-step reaction with 3 steps

1.1: NaH; tetra-n-butylammonium chloride / dimethylformamide / 0.5 h / 0 °C

1.2: 84 percent / dimethylformamide / 4 h

2.1: 89 percent / stannous chloride / methanol / 20 °C

3.1: 89 percent / Ph₃P; imidazole; I₂ / diethyl ether / 0 °C

With 1H-imidazole; tetrabutyl-ammonium chloride; iodine; sodium hydride; triphenylphosphine; tin(ll) chloride; In methanol; diethyl ether; N,N-dimethyl-formamide;

Reference yield:

: 629-30-1
1,7-heptandiol

: 370863-08-4
7-benzyloxy-1-iodooctane

Guidance literature:: Multi-step reaction with 6 steps

1.1: 75.53 percent / stannous chloride dihydrate / CHCl₃ / 24 h

2.1: 60.57 percent / CrO₃*pyridine / CHCl₃ / 0 °C

3.1: Mg / diethyl ether

3.2: 93 percent / diethyl ether / 0.5 h

4.1: NaH; tetra-n-butylammonium chloride / dimethylformamide / 0.5 h / 0 °C

4.2: 84 percent / dimethylformamide / 4 h

5.1: 89 percent / stannous chloride / methanol / 20 °C

6.1: 89 percent / Ph₃P; imidazole; I₂ / diethyl ether / 0 °C

With 1H-imidazole; chromium trioxide-pyridine complex; tetrabutyl-ammonium chloride; iodine; sodium hydride; magnesium; triphenylphosphine; tin(ll) chloride; In methanol; diethyl ether; chloroform; N,N-dimethyl-formamide; 3.1: Grignard reaction / 3.2: Grignard reaction;