Technology Process of 7-benzyloxyoctanol
There total 5 articles about 7-benzyloxyoctanol which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
tin(ll) chloride;
In
methanol;
at 20 ℃;
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: NaH; tetra-n-butylammonium chloride / dimethylformamide / 0.5 h / 0 °C
1.2: 84 percent / dimethylformamide / 4 h
2.1: 89 percent / stannous chloride / methanol / 20 °C
With
tetrabutyl-ammonium chloride; sodium hydride; tin(ll) chloride;
In
methanol; N,N-dimethyl-formamide;
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: 75.53 percent / stannous chloride dihydrate / CHCl3 / 24 h
2.1: 60.57 percent / CrO3*pyridine / CHCl3 / 0 °C
3.1: Mg / diethyl ether
3.2: 93 percent / diethyl ether / 0.5 h
4.1: NaH; tetra-n-butylammonium chloride / dimethylformamide / 0.5 h / 0 °C
4.2: 84 percent / dimethylformamide / 4 h
5.1: 89 percent / stannous chloride / methanol / 20 °C
With
chromium trioxide-pyridine complex; tetrabutyl-ammonium chloride; sodium hydride; magnesium; tin(ll) chloride;
In
methanol; diethyl ether; chloroform; N,N-dimethyl-formamide;
3.1: Grignard reaction / 3.2: Grignard reaction;