2H-1,3,4-Oxadiazin-2-one, 3,6-dihydro-3,5,6-triphenyl-

Base Information

Chemical Name:2H-1,3,4-Oxadiazin-2-one, 3,6-dihydro-3,5,6-triphenyl-
CAS No.:380600-37-3
Molecular Formula:C21H16N2O2
Molecular Weight:328.37
Hs Code.:

Synonyms:

Suppliers and Price of 2H-1,3,4-Oxadiazin-2-one, 3,6-dihydro-3,5,6-triphenyl-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 2H-1,3,4-Oxadiazin-2-one, 3,6-dihydro-3,5,6-triphenyl-

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 2H-1,3,4-Oxadiazin-2-one, 3,6-dihydro-3,5,6-triphenyl-

There total 6 articles about 2H-1,3,4-Oxadiazin-2-one, 3,6-dihydro-3,5,6-triphenyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 2-phenylacetophenone N-(carboethoxy)-N-phenylhydrazone

: 380600-37-3
3,5,6-triphenyl-3,6-dihydro-1-oxa-3,4-diazin-2-one

Guidance literature:: With phenyltrimethylammonium tribromide; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1021/ol025587w

Reference yield:

: 6121-47-7
2-phenylacetophenone phenylhydrazone

: 380600-37-3
3,5,6-triphenyl-3,6-dihydro-1-oxa-3,4-diazin-2-one

Guidance literature:: Multi-step reaction with 2 steps

1: 66 percent / n-butyl lithium / tetrahydrofuran; hexane / -78 - 20 °C

2: 91 percent / phenyltrimethylammonium tribromide / tetrahydrofuran; dimethylformamide

With n-butyllithium; phenyltrimethylammonium tribromide; In tetrahydrofuran; hexane; N,N-dimethyl-formamide;
DOI:10.1021/ol025587w

Reference yield:

: 451-40-1
phenyl benzyl ketone

: 380600-37-3
3,5,6-triphenyl-3,6-dihydro-1-oxa-3,4-diazin-2-one

Guidance literature:: Multi-step reaction with 3 steps

1: 93 percent / NaOAc trihydrate / acetic acid / 12 h / 20 °C

2: 66 percent / n-butyl lithium / tetrahydrofuran; hexane / -78 - 20 °C

3: 91 percent / phenyltrimethylammonium tribromide / tetrahydrofuran; dimethylformamide

With n-butyllithium; sodium acetate; phenyltrimethylammonium tribromide; In tetrahydrofuran; hexane; acetic acid; N,N-dimethyl-formamide;
DOI:10.1021/ol025587w