Benzenamine, 4-[bis(2,4,6-trimethylphenyl)boryl]-N,N-dimethyl-

Base Information

Chemical Name:Benzenamine, 4-[bis(2,4,6-trimethylphenyl)boryl]-N,N-dimethyl-
CAS No.:38186-30-0
Molecular Formula:C26H32BN
Molecular Weight:369.35000
Hs Code.:
Mol file:38186-30-0.mol

Synonyms:[p-(N,N-dimethylamino)phenyl]dimesitylborane;dimesityl(4-dimethylaminophenyl)borane;4-(dimesitylboryl)-N,N-dimethylaniline;Dimesityl(4-dimethylaminophenyl)boran;Benzenamine,4-[bis(2,4,6-trimethylphenyl)boryl]-N,N-dimethyl;

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Benzenamine, 4-[bis(2,4,6-trimethylphenyl)boryl]-N,N-dimethyl-

Chemical Property:

PSA：3.24000
LogP:4.11920

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Benzenamine, 4-[bis(2,4,6-trimethylphenyl)boryl]-N,N-dimethyl-

There total 5 articles about Benzenamine, 4-[bis(2,4,6-trimethylphenyl)boryl]-N,N-dimethyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 586-77-6
4-bromo-N,N-dimethylaniline

: 436-59-9
dimesitylfluoroborane

: 38186-30-0
[p-(N,N-dimethylamino)phenyl]dimesitylborane

Guidance literature:: 4-bromo-N,N-dimethylaniline; With n-butyllithium; In hexane; at 20 ℃; for 14h;

dimesitylfluoroborane; In diethyl ether; at 20 ℃; for 3h; Further stages.;
DOI:10.1002/chem.200501096

Reference yield: 50.0%

: 586-77-6
4-bromo-N,N-dimethylaniline

: 440361-72-8
(diphenylmethylsilyl)dimesitylborane

: 38186-30-0
[p-(N,N-dimethylamino)phenyl]dimesitylborane

Guidance literature:: With sodium t-butanolate; In 1,4-dioxane; hexane; at 50 ℃; for 24h; Inert atmosphere;
DOI:10.1002/chem.201604021

Reference yield:

: 436-59-9
dimesitylfluoroborane

: 38186-30-0
[p-(N,N-dimethylamino)phenyl]dimesitylborane

Guidance literature:: Multi-step reaction with 2 steps

1: tetrahydrofuran / 10 h / -60 - 20 °C / Inert atmosphere

2: sodium t-butanolate / 1,4-dioxane; hexane / 24 h / 50 °C / Inert atmosphere

With sodium t-butanolate; In tetrahydrofuran; 1,4-dioxane; hexane;
DOI:10.1002/chem.201604021