Benzenesulfonamide, N-[4,5-dimethoxy-2-(4-methylbenzoyl)phenyl]-4-methyl-

Base Information

Chemical Name:Benzenesulfonamide, N-[4,5-dimethoxy-2-(4-methylbenzoyl)phenyl]-4-methyl-
CAS No.:383895-73-6
Molecular Formula:C23H23NO5S
Molecular Weight:425.49700
Hs Code.:
Mol file:383895-73-6.mol

Synonyms:N-[4,5-Dimethoxy-2-(4-methyl-benzoyl)-phenyl]-4-methyl-benzenesulfonamide;

Suppliers and Price of Benzenesulfonamide, N-[4,5-dimethoxy-2-(4-methylbenzoyl)phenyl]-4-methyl-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Benzenesulfonamide, N-[4,5-dimethoxy-2-(4-methylbenzoyl)phenyl]-4-methyl-

Chemical Property:

Melting Point:195 - 196 °C (hexane)
PSA：90.08000
LogP:5.50620

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

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Technology Process of Benzenesulfonamide, N-[4,5-dimethoxy-2-(4-methylbenzoyl)phenyl]-4-methyl-

There total 5 articles about Benzenesulfonamide, N-[4,5-dimethoxy-2-(4-methylbenzoyl)phenyl]-4-methyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 98-59-9
p-toluenesulfonyl chloride

: 391251-83-5
(2-amino-4,5-dimethoxyphenyl)-(4-methylphenyl)methanone

: 383895-73-6
4,5-dimethoxy-2-(4-methylbenzoyl)-1-(4-methylphenylsulfonamido)benzene

Guidance literature:: With pyridine; at 20 ℃; for 1h;
DOI:10.1016/j.tet.2006.10.056

Reference yield:

: 681470-02-0
(4,5-dimethoxy-2-nitrophenyl)-(4-methylphenyl)methanone

: 383895-73-6
4,5-dimethoxy-2-(4-methylbenzoyl)-1-(4-methylphenylsulfonamido)benzene

Guidance literature:: Multi-step reaction with 2 steps

1: 73 percent / Fe; AcOH / H₂O; ethyl acetate / 6 h / Heating

2: 80 percent / pyridine / 1 h / 20 °C

With pyridine; iron; acetic acid; In water; ethyl acetate;
DOI:10.1016/j.tet.2006.10.056

Reference yield:

: 91-16-7
1,2-dimethoxybenzene

: 383895-73-6
4,5-dimethoxy-2-(4-methylbenzoyl)-1-(4-methylphenylsulfonamido)benzene

Guidance literature:: Multi-step reaction with 4 steps

1: AlCl₃ / benzene / 2.5 h / 55 - 60 °C

2: 68 percent / HNO₃; AcOH / 0.5 h / 0 - 20 °C

3: 73 percent / Fe; AcOH / H₂O; ethyl acetate / 6 h / Heating

4: 80 percent / pyridine / 1 h / 20 °C

With pyridine; aluminium trichloride; nitric acid; iron; acetic acid; In water; ethyl acetate; benzene; 1: Friedel-Crafts reaction;
DOI:10.1016/j.tet.2006.10.056